Jove Lab Chem

Lab 60: Synthesis of Luminol — Materials List

Preparation for 10 Students

• Stirring hotplate
  5
• Bunsen burner with tubing and striker
  5
• Lab Stand
  10
• 3-prong clamp
  15
• Insulated gloves or flask tongs
  5
• 10-mL glass graduated cylinder
  20
• 50-mL glass graduated cylinder
  5
• 25-mL Erlenmeyer flask
  15
• 250-mL glass filter flask
  5
• 50-mL glass beaker
  5
• 250-mL glass beaker
  10
• 400-mL glass beaker
  5
• 600-mL glass beaker
  5
• 25-mL glass test tube
  10
• Büchner funnel
  10
• Long glass stirring rod
  5
• Medium stir bar
  5
• Thermometers
  10
• Spatulas
  10
• Boiling chips
  30
• Medium filter adapter
  5
• Test tube stopper
  5
• Stopper for 25-mL Erlenmeyer flask
  5
• Tweezers
  5
• Laboratory tape
  5 rolls
• Labeling pen or marker
  5
• Pipette bulbs
  10
• Circular filter paper (9-mm)
  10
• Hydrazine hydrate (64% hydrazine)
  5 mL
• Sodium hydroxide
  5 g
• 3-nitrophthalic acid
  5 g
• Triethylene glycol
  25 mL
• Anhydrous sodium dithionite
  20 g
• Glacial acetic acid
  15 mL
• Potassium hydroxide
  5 g
• Dimethyl sulfoxide
  20 mL
• Fluorescein sodium salt
  2 g
• 10 wt% sodium hypochlorite solution
  300 mL
• 1 M sodium carbonate
  100 mL
• 1-mL graduated pipette and pipette controller
  1
• 10-mL glass graduated cylinder
  2
• 50-mL glass graduated cylinder
  1
• 30-mL glass beaker
  1
• 50-mL glass beaker
  1
• 20-mL glass bottle with cap
  2
• Test tube brush
  2
• 250-mL wash bottle filled with DI water
  Dependent on lab size
• Crushed ice
  Dependent on lab size
• Ice scoop
  Dependent on lab size
• Insulated ice cooler
  Dependent on lab size
• Analytical balance (at least 1)
  Dependent on lab size
• Weigh boats (at least 5 per group)
  Dependent on lab size
• Spatulas
  Dependent on lab size
• Lab wipes
  Dependent on lab size
• Deionized water
  Dependent on lab size
• Pasteur pipettes
  Dependent on lab size
• Paraffin film
  Dependent on lab size
• Scissors
  Dependent on lab size