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Real-time Monitoring of Reactions Performed Using Continuous-flow Processing
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Real-time Monitoring of Reactions Performed Using Continuous-flow Processing: The Preparation of 3-Acetylcoumarin as an Example

Article DOI: 10.3791/52393-v • 09:56 min • November 18th, 2015
November 18th, 2015 •
1, 1
1Department of Chemistry, University of Connecticut

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Summary
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Real-time monitoring allows for fast optimization of reactions performed using continuous-flow processing. Here the preparation of 3-acetylcoumarin is used as an example. The apparatus for performing in-situ Raman monitoring is described, as are the steps required to optimize the reaction.

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Real-time Monitoring Reactions Continuous-flow Processing Optimization Inline Monitoring Product Quality Raman Spectrometer Flow Unit Back-pressure Regulator Atmospheric Pressure Tubing RT (room Temperature) Isothermal Conditions Chemical Reaction Piperidine-catalyzed Synthesis 3-acetylcoumarin Salicylaldehyde Ethyl Acetoacetate Flow Rates Temperatures
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