Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

Saeed Mozaffari; Wenhui Li; Coogan Thompson; Sergei Ivanov; Soenke Seifert; Byeongdu Lee; Libor Kovarik; Ayman M. Karim

doi:10.3791/57667

Journal

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化学

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Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

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JoVE 杂志化学

Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

DOI:

10.3791/57667-v

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11:54 min

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June 25, 2018

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Saeed Mozaffari*¹, Wenhui Li*¹, Coogan Thompson, Sergei Ivanov, Soenke Seifert, Byeongdu Lee, Libor Kovarik, Ayman M. Karim

¹Department of Chemical Engineering,Virginia Polytechnic Institute and State University, ²Center for Integrated Nanotechnologies,Los Alamos National Laboratory, ³Advanced Photon Source,Argonne National Laboratory, ⁴X-ray Science Division,Argonne National Laboratory, ⁵Environmental Molecular Science Laboratory,Pacific Northwest National Laboratory

Chapters

00:04Title
00:44Palladium(II) Acetate Recrystallization
03:54Colloidal Pd Nanoparticle Synthesis in Pyridine
06:25Pd Nanoparticle Characterization by Ex Situ Small-Angle X-Ray Scattering (SAXS)
09:52Results: Kinetics of Nucleation and Growth of Pd Nanoparticles in Toluene and Pyridine
11:20Conclusion

Summary

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The main goal of this work is to elucidate the role of capping agents in regulating the size of palladium nanoparticles by combining in situ small angle x-ray scattering (SAXS) and ligand-based kinetic modeling.

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Ligand-Mediated Nucleation and Growth of Palladium Metal Nanoparticles

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