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Manglende Analyse af batterier Brug Synchrotronbestrålingscenter-baserede Hard røntgen Microtomography

Published: August 26, 2015 doi: 10.3791/53021
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1,2, 3, 2,4,5
1Department of Materials Science and Engineering, University of California Berkeley, 2Materials Science Division, Lawrence Berkeley National Laboratory, 3Advanced Light Source Division, Lawrence Berkeley National Laboratory, 4Department of Chemical and Biomolecular Engineering, University of California Berkeley, 5Environmental Energy Technology Division, Lawrence Berkeley National Laboratory

Materials

Name Company Catalog Number Comments
Anhydrous N-methyl-2-pyrrolidone  MILLIPORE MX1396-7
Lithium bis(trifluoromethane)sulfonamide MILLIPORE 8438730010
Lithium metal FMC Lithium None Lectro Max 100
Pouch material MTI Corporation EQ-alf-400-7.5M
Nickel tabs MTI Corporation EQ-PLiB-NTA3

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References

  1. Bruce, P. G., Freunberger, S. A., Hardwick, L. J., Tarascon, J. M. Li-O-2 and Li-S batteries with high energy storage. Nat Mater. 11, 19-29 (2012).
  2. Balsara, N. P., Newman, J. Comparing the Energy Content of Batteries, Fuels, and Materials. J Chem Educ. 90, 446-452 (2013).
  3. Girishkumar, G., McCloskey, B., Luntz, A. C., Swanson, S., Wilcke, W. Lithium - Air Battery: Promise and Challenges. J Phys Chem Lett. 1, 2193-2203 (2010).
  4. Selim, R., Bro, P. Some observations on rechargeable lithium electrodes in a propylene carbonate electrolyte. J Electrochem Soc. 121, 1457-1459 (1974).
  5. Aurbach, D., Zinigrad, E., Cohen, Y., Teller, H. A short review of failure mechanisms of lithium metal and lithiated graphite anodes in liquid electrolyte solutions. Solid State Ionics. 148, 405-416 (2002).
  6. Monroe, C., Newman, J. Dendrite Growth in Lithium/Polymer Systems. J Electrochem Soc. 150, A1377 (2003).
  7. Barton, J. L., Bockris, J. O. The Electrolytic Growth of Dendrites from Ionic Solutions. Proc R Soc Ser A. 268, 485-505 (1962).
  8. Bhattacharyya, R., et al. In situ NMR observation of the formation of metallic lithium microstructures in lithium batteries. Nat Mater. 9, 504-510 (2010).
  9. Chandrashekar, S., et al. 7Li MRI of Li batteries reveals location of microstructural lithium. Nat Mater. 11, 311-315 (2012).
  10. Arora, P., White, R. E., Doyle, M. Capacity fade mechanisms and side reactions in lithium-ion batteries. J Electrochem Soc. 145, 3647-3667 (1998).
  11. Ebner, M., Marone, F., Stampanoni, M., Wood, V. Visualization and Quantification of Electrochemical and Mechanical Degradation in Li Ion Batteries. Science. 342, 716-720 (2013).
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  14. Shui, J. -L., et al. Reversibility of anodic lithium in rechargeable lithium–oxygen batteries. Nat commun. 4, (2013).
  15. Harry, K. J., Hallinan, D. T., Parkinson, D. Y., MacDowell, A. A., Balsara, N. P. Detection of subsurface structures underneath dendrites formed on cycled lithium metal electrodes. Nat Mater. 13, 69-73 (2014).
  16. Baruchel, J., et al. Advances in synchrotron hard X-ray based imaging. Cr Phys. 9, 624-641 (2008).
  17. Flannery, B. P., Deckman, H. W., Roberge, W. G., D'Amico, K. L. Three-Dimensional X-ray Microtomography. Science. 237, 1439-1444 (1987).
  18. Singh, M., et al. Effect of molecular weight on the mechanical and electrical properties of block copolymer electrolytes. Macromolecules. 40, 4578-4585 (2007).
  19. Monroe, C., Newman, J. The Impact of Elastic Deformation on Deposition Kinetics at Lithium/Polymer Interfaces. J Electrochem Soc. 152, A396-1149 (2005).
  20. Stone, G. M., et al. Resolution of the Modulus versus Adhesion Dilemma in Solid Polymer Electrolytes for Rechargeable Lithium Metal Batteries. J Electrochem Soc. 159, A222-A227 (2012).
  21. Panday, A., et al. Effect of Molecular Weight and Salt Concentration on Conductivity of Block Copolymer Electrolytes. Macromolecules. 42, 4632-4637 (2009).
  22. Avizo v.8.1. , FEI Company. Hillsboro, Oregon. Available from: http://www.vsg3d.com/ (2014).
  23. Schneider, C. A., Rasband, W. S., Eliceiri, K. W. NIH Image to ImageJ: 25 years of image analysis. Nat methods. 9, 671-675 (2012).
  24. Henke, B. L., Gullikson, E. M., Davis, J. C. X-Ray Interactions - Photoabsorption, Scattering, Transmission and Reflection at E=50-30,000 Ev, Z=1-92 (Vol 54, Pg 181, 1993). Atom Data Nucl Data. 55, 349-349 (1993).
Manglende Analyse af batterier Brug Synchrotronbestrålingscenter-baserede Hard røntgen Microtomography
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Harry, K. J., Parkinson, D. Y.,… More

Harry, K. J., Parkinson, D. Y., Balsara, N. P. Failure Analysis of Batteries Using Synchrotron-based Hard X-ray Microtomography. J. Vis. Exp. (102), e53021, doi:10.3791/53021 (2015).

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