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Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques

Article DOI: 10.3791/50594-v • 10:03 min • November 11th, 2013
November 11th, 2013 •
1, 1, 1,2, 1, 3, 1, 1, 1, 4, 5
1Environmental Energy Technologies Division, Lawrence Berkeley National Laboratory, 2Department of Chemistry, University of Illinois at Chicago, 3Stanford Synchrotron Radiation Lightsource, 4Haldor Topsøe A/S, 5PolyPlus Battery Company

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We describe the use of synchrotron X-ray absorption spectroscopy (XAS) and X-ray diffraction (XRD) techniques to probe details of intercalation/deintercalation processes in electrode materials for Li-ion and Na-ion batteries. Both in situ and ex situ experiments are used to understand structural behavior relevant to the operation of devices

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Electrode Materials Lithium-ion Batteries Sodium-ion Batteries Synchrotron Radiation Techniques Intercalation Compounds Transition Metal Oxides Transition Metal Phosphates Redox States Structural Transformations Phase Transitions Lattice Parameter Changes Potential Profiles Rate Capabilities Cycle Lives X-ray Diffraction (XRD) X-ray Absorption Spectroscopy (XAS) In Situ Experiments Electrochemical Properties Structural Properties
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