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JoVE Journal Chemistry
Syntese og karakterisering af funktionaliserede Metal-organisk Frameworks
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Syntese og karakterisering af funktionaliserede Metal-organisk Frameworks

Article DOI: 10.3791/52094-v • 11:27 min • September 5th, 2014
September 5th, 2014 •
1, 1,2, 1, 1, 1,3
1Department of Chemistry, Northwestern University, 2Department of Chemistry, Warsaw University of Technology, 3Department of Chemistry, Faculty of Science, King Abdulaziz University

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Syntese, aktivering, og karakterisering af bevidst designede metal-økologiske rammebetingelser materialer er udfordrende, især når byggesten er inkompatible eller uønskede polymorfe er termodynamisk begunstiget i de ønskede former. Vi beskriver, hvordan applikationer opløsningsmiddel-assisteret udveksle linker, pulver røntgendiffraktion i kapillærer og aktivering via superkritisk CO 2 tørring, kan løse nogle af disse udfordringer.

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Kemi Metal-organisk rammer porøse koordinationscentre polymerer superkritisk CO krystallografi solvothermal sorption solvent-assisteret udveksle linker
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