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Synthesis of Ligand-free CdS Nanoparticles within a Sulfur Copolymer Matrix
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Synthesis of Ligand-free CdS Nanoparticles within a Sulfur Copolymer Matrix

Article DOI: 10.3791/54047-v • 09:15 min • May 1st, 2016
May 1st, 2016 •
1,2,3, 4, 2,3,5, 1,2,3,6
1Department of Materials Science and Engineering, University of Washington, 2Molecular Engineering and Sciences Institute, University of Washington, 3Clean Energy Institute, University of Washington, 4Institut für Nanospektroskopie, Helmholtz-Zentrum Berlin für Materialien und Energie GmbH, 5Department of Chemical Engineering, University of Washington, 6Department of Chemistry, University of Washington

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Summary
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Herein we present a method to synthesize ligand-free cadmium sulfide (CdS) nanoparticles based on a unique sulfur copolymer. The sulfur copolymer operates as a high temperature solvent and a sulfur source during the nanoparticle synthesis and stabilizes the nanoparticles after the reaction.

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Ligand-free CdS Nanoparticles Sulfur Copolymer Matrix Synthesis Method Nanoparticle Surface Modification Reactions Aliphatic Ligands Range Of Fields Nanoparticle Ligands Molten Elemental Sulfur 15 Milliliter Three-neck Flask Pump And Purge Cycles Alpha-methylstyrene Copolymer Formation Solution Color Change Orange Rubbery Solid
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