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Utarbeidelse av DMMTAV og DMDTAV bruker DMAV for miljømessige programmer
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Utarbeidelse av DMMTAV og DMDTAV bruker DMAV for miljømessige programmer: syntese, rensing og bekreftelse

Article DOI: 10.3791/56603-v • 06:23 min • March 9th, 2018
March 9th, 2018 •
1, 2, 1, 1
1Korea Basic Science Institute, Seoul Center, 2Natural Science Research Institute, Yonsei University

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Denne artikkelen presenterer endret eksperimentelle protokoller for dimethylmonothioarsinic syre (DMMTAV) og dimethyldithioarsinic syre (DMDTAV) syntese, inducing dimethylarsinic syre (DMAV) thiolation gjennom blanding av DMAV , Na2S og H2så4. Endret protokollen inneholder en eksperimentell retningslinjer, dermed overvinne begrensninger av syntese trinnene som kan ha forårsaket eksperimentelle feil i kvantitativ analyse.

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Miljøfag problemet 133 Dimethylated thioarsenicals dimethylmonothioarsinic acid dimethyldithioarsinic syre syntese HPLC-ICP-MULTIPLE Sclerosis ESI-MS
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