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Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate
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Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate

Article DOI: 10.3791/57233-v • 06:18 min • April 24th, 2018
April 24th, 2018 •
1, 1, 1
1Centro de Química, Instituto de Ciencias, Benemérita Universidad Autónoma de Puebla

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Herein, we report the synthesis and crystallization of 3,5-lutidine N-oxide dehydrate by a simple protocol that differs from the classical synthesis of pyridine N-oxide. This protocol utilizes different starting material and involves less reaction time to yield a new solvated supramolecular structure, which crystallizes under slow evaporation.

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Synthesis Crystallization Spectroscopic Characterization 3,5-lutidine N-oxide Dehydrate X-ray Monocrystals Solvated Supramolecular Structure Synthetic Organic Chemistry Inorganic Chemistry Noble Aromatic Compounds Et-see-cic Compounds Perioding Dare-ee-batics Research Laboratory Optimal Route Glacial Acetic Acid 3,5-dimethylpyridine Hydrogen Peroxide Reaction Mixture Inner Temperature High-vacuum Distillation Unit Excess Acetic Acid Distilled Water
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