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JoVE Journal Chemistry
Regioselective O- glykosylering av Nucleosides via den midlertidige 2', 3-Diol beskyttelse av en Boronic Ester for syntese av smakløst Nucleosides
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Regioselective O- glykosylering av Nucleosides via den midlertidige 2', 3-Diol beskyttelse av en Boronic Ester for syntese av smakløst Nucleosides

Article DOI: 10.3791/57897-v • 08:46 min • July 26th, 2018
July 26th, 2018 •
1, 1, 1, 1,2
1Faculty of Pharmaceutical Sciences, Tokyo University of Science, 2Imaging Frontier Center, Tokyo University of Science

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Her presenterer vi protokoller for syntese av smakløst nucleosides av regioselective O- glykosylering av ribonucleosides via en midlertidig beskyttelse av deres 2, 3-diol moieties utnytte en syklisk boronic ester. Denne metoden gjelder flere ubeskyttet nucleosides som adenosin, guanosine, cytidine, uridine, 5-methyluridine og 5-fluorouridine å gi tilsvarende smakløst nucleosides.

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Kjemi problemet 137 smakløst nucleosides O- glykosylering ribonucleosides midlertidig beskyttelse thioglycosides syklisk boronic ester
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