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Journal / Chemistry / Solid-fase syntese av [4.4] Spirocyclic Oximes
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JoVE Journal Chemistry
Solid-fase syntese av [4.4] Spirocyclic Oximes
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Solid-fase syntese av [4.4] Spirocyclic Oximes

Article DOI: 10.3791/58508-v • 05:15 min • February 6th, 2019
February 6th, 2019 •
1, 1, 1
1Department of Biology and Chemistry, Azusa Pacific University

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Her presenterer vi en protokoll for å demonstrere en effektiv metode for syntese av spirocyclic heterocycles. Fem-trinns prosess benytter solid-fase syntese og regenererende Michael koblingsfunksjonalitet strategier. Generelt vanskelig å syntetisere, presenterer vi en passelig metode for syntese av spirocyclic molekyler ellers utilgjengelige for andre moderne tilnærminger.

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Kjemi problemet 144 Solid-fase syntese regenererer Michael linker intramolekylære 1,3-dipolar cycloaddition spirocyclic heterocycles trisykliske middels høy diastereoselectivity
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