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Chemistry

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JoVE Journal Chemistry
Isolera gratis Karbener, deras blandade dimerer och organiska radikaler
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Isolera gratis Karbener, deras blandade dimerer och organiska radikaler

Article DOI: 10.3791/59389-v • 10:44 min • April 19th, 2019
April 19th, 2019 •
1, 1, 1
1Department of Chemistry and Pharmacy, Friedrich-Alexander-Universität Erlangen-Nürnberg

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Vi presenterar protokoll för isolering av stabil heterocykliska karbener. Syntesen av en cyklisk (alkyl)(amino) Karben (CAAC) och en N-heterocykliska Karben (NHC) demonstreras med hjälp av filtret kanyler och Schlenk teknik. Dessutom presenterar vi syntesen av den relaterade syre-känsligt, elektron-rika blandade ”Wanzlick dimer” och minskad stabila organiska radikalen.

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Fråga 146 karbener kemi kemi N-heterocykliska Karben NHC cykliska (alkyl)(amino) Karben CAAC filter kanyl Schlenk teknik air känslig Wanzlicks jämvikt ekologiska radikala elektron-rika olefiner
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