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JoVE Journal Chemistry
Vorbereitung von graphengestützten Microwell Liquid Cells für die In Situ Transmission Electron Microscopy
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Vorbereitung von graphengestützten Microwell Liquid Cells für die In Situ Transmission Electron Microscopy

Article DOI: 10.3791/59751-v • 08:30 min • July 15th, 2019
July 15th, 2019 •
*1, *1, 2, 3, 3, 1,2,4
1Electron Devices (LEB), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg, 2Fraunhofer Institute for Integrated Systems and Device Technology (IISB), 3Institute of Micro- and Nanostructure Research (IMN) and Center for Nanoanalysis and Electron Microscopy (CENEM), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg, 4Power Electronics (LEE), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg
* These authors contributed equally

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Ein Protokoll zur Herstellung von graphengestützten Mikrowell-Flüssigkeitszellen für die In-situ-Elektronenmikroskopie von Gold-Nanokristallen aus der HAuCl 4-Vorläuferlösung wird vorgestellt. Darüber hinaus wird eine Analyseroutine zur Quantifizierung der beobachteten Radierung und Wachstumsdynamik vorgestellt.

Tags

Chemie Ausgabe 149 Flüssigzelle in situ TEM Nanopartikel Synthese Ätzen Wachstum Gold Kinetik Graphen Dendrit Einzelpartikelverfolgung
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