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Linjeformanalyse af dynamiske NMR-spektre til karakterisering af koordinationssfæreomlejringer ved et chiralt rheniumpolyhydridkompleks
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Linjeformanalyse af dynamiske NMR-spektre til karakterisering af koordinationssfæreomlejringer ved et chiralt rheniumpolyhydridkompleks

Article DOI: 10.3791/64160-v • 10:52 min • July 27th, 2022
July 27th, 2022 •
1, 1, 1, 1
1Department of Chemistry and Physics, Monmouth University

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Linjeformanalyse af NMR-spektre indsamlet over en række temperaturer tjener som vejledning til omlejring af indre koordinatkugleatomer ved et chiralt, otte-koordinat, rhenium (V) polyhydridkompleks, ReH5 (PPh 3) 2 (sek-butylamin). Linjeformanalyse bruges også til at bestemme aktiveringsparametrene ΔH‡, ΔS‡ og ΔG‡ for disse atomomlejringer.

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