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이 동영상은 전자 충격 이온화를 사용하여 휘발성 산화에 민감한 화합물의 질량 spectrometrical 분석을위한 프로토콜을 제공합니다. 제시된 기법은 금속 organyls 실란, 또는 쉬 렝크 기법 불활성 조건을 이용하여 처리하는 것이 필요 phosphanes 작업, 특히 무기 화학자 관심사이다.