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JoVE Journal Chemistry
Tilgang Valuable Ligand Støtter for Transition Metals
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Tilgang Valuable Ligand Støtter for Transition Metals: En modifisert, Intermediate Scale Utarbeidelse av 1,2,3,4,5-Pentamethylcyclopentadiene

Article DOI: 10.3791/55366-v • 09:45 min • March 20th, 2017
March 20th, 2017 •
1, 1, 1
1Department of Science, Mount St. Mary's University

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Pålitelig, middels skala utarbeidelse av 1,2,3,4,5-pentamethylcyclopentadiene (Cp * H) er presentert. Den reviderte protokollen for syntese og rensing av liganden minimerer behovet for spesialisert laboratorieutstyr samtidig forenkle reaksjons workups og produktrensing. Bruk av Cp * H i syntesen av [Cp * MCL 2] 2-komplekser (M = Ru, Ir) er også beskrevet.

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Kjemi Cp * H Iridium ligand Pentamethylcyclopentadiene ruthenium syntese Transition Metals
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