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Characterization of Synthetic Polymers via Matrix Assisted Laser Desorption Ionization Time of Flight (MALDI-TOF) Mass Spectrometry
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Characterization of Synthetic Polymers via Matrix Assisted Laser Desorption Ionization Time of Flight (MALDI-TOF) Mass Spectrometry

Article DOI: 10.3791/57174-v • 06:56 min • June 10th, 2018
June 10th, 2018 •
1, 1
1Department of Chemistry, Tulane University

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Summary
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A protocol for the matrix-assisted laser desorption ionization time of flight mass spectrometry (MALDI-TOF MS) characterization of synthetic polymers is described including the optimization of sample preparation, spectral acquisition, and data analysis.

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MALDI-TOF MS Synthetic Polymers Characterization Matrix-assisted Laser Desorption Ionization Time Of Flight Mass Spectrometry Sample Preparation Acquisition Analysis Molecular Weight Dispersity End Group Identity Homopolymer End Groups Solutions Matrix Analyte Cation Solutions Poly(L-lactide) 2,5-dihydroxybenzoic Acid Solution Sodium Trichloroacetate Solution MALDI Target Plate Data Acquisition Software Flexcontrol
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