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JoVE Journal Chemistry
Isolere gratis Carbenes samt blandede dimere og organiske radikaler
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Isolere gratis Carbenes samt blandede dimere og organiske radikaler

Article DOI: 10.3791/59389-v • 10:44 min • April 19th, 2019
April 19th, 2019 •
1, 1, 1
1Department of Chemistry and Pharmacy, Friedrich-Alexander-Universität Erlangen-Nürnberg

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Vi præsenterer protokoller til isolering af stabil Heterocycliske carbenes. Syntesen af et cyklisk (alkyl)(amino) carbene (CAAC) og et N-Heterocycliske carbene (NHC) er påvist ved hjælp af filter cannulas og Schlenk teknik. Desuden præsenterer vi syntesen af de relaterede ilt-følsomme, elektron-rige blandet "Wanzlick dimer" og den reducerede stabile organiske radikaler.

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Kemi spørgsmålet 146 kemi carbenes N-Heterocycliske carbene NHC cyklisk (alkyl)(amino) carbene CAAC filter kanyle Schlenk teknik air følsomme Wanzlicks ligevægt organiske radikal elektron-rige olefiner
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