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Journal / Chemistry / 微波辅助制备1-Aryl-1 H-pyrazole-5胺
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JoVE Journal Chemistry
微波辅助制备1-Aryl-1 H-pyrazole-5胺
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微波辅助制备1-Aryl-1 H-pyrazole-5胺

Article DOI: 10.3791/59896-v • 05:07 min • June 23rd, 2019
June 23rd, 2019 •
*1, *1, *1, 1
1Department of Chemistry and Biochemistry, California Polytechnic State University
* These authors contributed equally

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1-Aryl-1H-pyrazole-5-胺由丙烯氢化物制备,与使用微波反应器的1M HCl溶液中的3氨基克罗诺辛或β-氰酮结合制备。大多数反应在10-15分钟内完成,纯产品可以通过真空过滤获得,典型的隔离产量为70-90%。

Tags

化学 问题 148 pyrazole-5-胺 微波合成 异体循环 绿色化学 循环 苯甲酰胺 β-氰酮 3-氨基克罗诺辛
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