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JoVE Journal Chemistry
Preparazione a microonde di 1-Aryl-1H-pyrazole-5-ammine
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Preparazione a microonde di 1-Aryl-1H-pyrazole-5-ammine

Article DOI: 10.3791/59896-v • 05:07 min • June 23rd, 2019
June 23rd, 2019 •
*1, *1, *1, 1
1Department of Chemistry and Biochemistry, California Polytechnic State University
* These authors contributed equally

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1-Aryl-1H-pyrazole-5-ammine sono preparati da idrazine di aryl combinate con 3-aminocrotononitrile o un cannioketone in una soluzione HCl da 1 M utilizzando un reattore a microonde. La maggior parte delle reazioni sono fatte in 10-15 minuti e il prodotto puro può essere ottenuto tramite filtrazione sottovuoto con rese isolate tipiche del 70-90%.

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Chimica Numero 148 pirazola-5-ammine sintesi di microonde eterocicli chimica verde ciclolizzazione fenilidrazzina z-cianoketone 3-aminocrotononitrile
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