Supercritical Co2

Supercritical CO2 is carbon dioxide maintained above its critical temperature and pressure, where it exhibits both gas-like transport and liquid-like density, making it valuable as an engineering working fluid. Above 31.1 °C and 7.38 MPa, its density, viscosity, and solvent strength can be tuned by changing pressure and temperature, enabling efficient heat transfer and mass transport. Engineers use supercritical CO2 in closed Brayton power cycles, refrigeration, extraction, cleaning, and materials processing. These systems can reduce equipment size and improve energy efficiency, while ongoing research addresses turbomachinery design, corrosion, sealing, and high-pressure safety.

Supercritical Co2 - Related Videos

Research

JoVE Journal - Chemistry

Supercritical Nitrogen Processing for the Purification of Reactive Porous Materials

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Cited by 9 •

2015

Nitrogen is an effective supercritical fluid for extraction or drying processes due to its small molecular size, high density in the near-liquid supercritical regime, and chemical inertness. We present a supercritical nitrogen drying protocol for the purification treatment of reactive, porous materials.

Preparing Silica Aerogel Monoliths via a Rapid Supercritical Extraction Method

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Cited by 26 •

2014

This article describes a rapid supercritical extraction method for fabricating silica aerogels. By utilizing a confined mold and hydraulic hot press, monolithic aerogels can be made in eight hours or less.

Education

JoVE Core - Analytical Chemistry

Supercritical Fluid Chromatography

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2024

Supercritical fluid chromatography (SFC) provides a beneficial substitute for gas chromatography (GC) and liquid chromatography (LC) for certain samples because it merges the top attributes of both techniques. SFC allows the separation and analysis of compounds that GC or LC does not easily manage. These compounds are traditionally nonvolatile or thermally unstable, making GC unsuitable and lacking functional groups required for HPLC analysis. SFC utilizes a supercritical fluid mobile phase,...

Fabrication and Testing of Catalytic Aerogels Prepared Via Rapid Supercritical Extraction

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Cited by 6 •

2018

Here we present protocols for preparing and testing catalytic aerogels by incorporating metal species into silica and alumina aerogel platforms. Methods for preparing materials using copper salts and copper-containing nanoparticles are featured. Catalytic testing protocols demonstrate the effectiveness of these aerogels for three-way catalysis applications.

Microfluidic Fabrication Techniques for High-Pressure Testing of Microscale Supercritical CO2 Foam Transport in Fractured Unconventional Reservoirs

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Cited by 8 •

2020

This paper describes a protocol along with a comparative study of two microfluidic fabrication techniques, namely photolithography/wet-etching/thermal-bonding and Selective Laser-induced Etching (SLE), that are suitable for high-pressure conditions. These techniques constitute enabling platforms for direct observation of fluid flow in surrogate permeable media and fractured systems under reservoir conditions.

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