At the end of this lab, students should know...
溶解度描述了在溶剂中可以溶解多少溶质。这取决于溶质与溶剂之间的溶解过程,因此同一溶质在不同溶剂中的溶解度会有所不同。
系统的温度会影响溶解度。您应始终确认溶解度数值所对应的温度。溶解度通常随温度升高而增加,但也有例外情况。
“相似相溶”这一说法提醒我们,极性溶质通常在极性溶剂中溶解性良好,而在非极性溶剂中溶解性较差;而非极性溶质通常在非极性溶剂中溶解性良好,但在极性溶剂中溶解性较差。
在给定溶剂体积和温度的条件下,饱和溶液含有最大量的已溶解溶质。溶质...
来源:美国马里兰州约翰斯·霍普金斯大学 Smaa Koraym
此处展示的是供10名学生两两分组进行实验的准备方案,并包含少量余量。请根据实际需要调整用量。
| 1 铁架台 |
| 1 滴定管夹 |
| 1 50-mL玻璃滴定管 |
| 1 温度计夹 |
| 1 数字温度计 |
| 1 玻璃温度计 |
| 1 长柄漏斗 |
| 1 5-mL移液管 |
| 1 10-mL移液器 |
| 1 50-mL量筒 |
| 5 250-mL锥形瓶 |
| 2 400-mL烧杯 |
| 1 150-mL烧杯 |
| 1 搅拌加热板 |
| 1 搅拌子 |
View the full transcript and gain access to JoVE Lab Manual videos
Q1: What materials do you need to prepare for a borax solubility lab?
Each student pair requires a ring stand, burette clamp, 50-mL glass burette, thermometer clamp, digital and glass thermometers, long-stem funnel, volumetric pipette, pipetter, graduated cylinder, five 250-mL Erlenmeyer flasks, two 400-mL beakers, one 150-mL beaker, and a stirring hotplate with stir bar for heating and mixing solutions.
Q2: How do you prepare a 0.5 M HCl solution for the borax experiment?
Using a volumetric pipette, transfer 20 mL of concentrated HCl to a 500-mL volumetric flask. Dilute the solution to the 500-mL mark with deionized water and mix on a stir plate until homogeneous. Store the prepared solution in an appropriate bottle until the lab session begins.
Q3: Why are different temperatures assigned to lab groups in a solubility experiment?
Assigning each group a specific temperature—10, 20, 30, 40, or 50 °C—allows students to collect solubility data across a temperature range. This approach enables the class to generate a complete solubility curve showing how borax solubility changes with temperature, providing comprehensive experimental data.
Q4: What is the role of bromocresol green indicator in the borax solubility lab?
Bromocresol green indicator is prepared as a 0.1% solution in dropper bottles, one per lab group. It serves as a visual indicator to detect the endpoint during titration, changing color when the acid-base reaction reaches completion, allowing students to accurately determine borax concentration.
Q5: How should you set up the weigh station for borax preparation?
Place a stock bottle of borax, weighing boats, and a spatula at each weigh station. This setup allows students to accurately measure and transfer the required mass of borax for their assigned temperature. Ensure adequate space and organization so multiple groups can weigh samples simultaneously without cross-contamination.
Q6: What is the purpose of using a volumetric pipette in HCl solution preparation?
A volumetric pipette delivers a precise volume of concentrated HCl—exactly 20 mL—ensuring accurate dilution to create a standardized 0.5 M solution. This precision is critical for reproducible experimental results and allows all lab groups to work with identically prepared acid solutions.