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Obtaining 3D Chemical Maps by Energy Filtered Transmission Electron Microscopy Tomography

Article DOI: 10.3791/56671-v • 08:15 min • June 9th, 2018
June 9th, 2018 •
1, 2, 3, 3
1Univ Lyon, INSA-Lyon, Université Claude Bernard Lyon 1, 2IFP Energies nouvelles, 3Institut de Physique et Chimie des Matériaux de Strasbourg (IPCMS)

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This paper describes a protocol to achieve 3D chemical maps combining energy filtered imaging and electron tomography. The chemical distribution of two catalyst supports formed by elements that are difficult to distinguish by other imaging techniques was studied. Each application consists of mapping overlapped chemical elements - respectively spaced-ionization edges.

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3D Chemical Maps Energy Filtered Transmission Electron Microscopy Tomography Material Science Chemistry Catalysis Fields Nanometric Scale Chemical Distribution Surface Analysis Energy Filtered Imaging Chemical Elements Experimental Protocol Quantification Of Chemical Parameters Beam Sensitivity Sample Preparation Electron Microscope Tilt Series Search Chemical Element Image Analysis EFTEMTomoJ Plugin
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