At the end of this lab, students should know...
용해도 (Solubility)는 용질이 용매에 얼마나 많이 용해 될 수 있는지를 나타냅니다. 이것은 용질과 용매 사이의 용해 과정에 따라 달라지므로 용질은 다른 용매에서 다른 용해도를 갖습니다.
용해도는 시스템의 온도에 영향을받습니다. 용해도 값과 관련된 온도를 항상 확인해야 합니다. 용해도는 일반적으로 온도에 따라 증가하지만 예외가 있습니다.
"like dissolves like"라는 문구는 극성 용질은 일반적으로 극성 용매에 대한 용해도가 좋고 비극성 용매에 대한 용해도가 낮은 반면...
출처: Smaa Koraym at Johns Hopkins University, MD, USA
여기에서는 10명의 학생이 짝을 지어 작업하는 실험실 준비 과정을 보여주며, 약간의 과잉이 있습니다. 필요에 따라 수량을 조정하십시오.
| 1 링 스탠드 |
| 1 뷰렛 클램프 |
| 1 50mL 유리 뷰렛 |
| 1 온도계 클램프 |
| 1 디지털 온도계 |
| 1 유리 온도계 |
| 1 긴 줄기 깔때기 |
| 1 5mL 부피 피펫 |
| 1 10mL 용량 피펫 |
| 1 50mL 눈금 실린더 |
| 5 250mL 삼각 플라스크 |
| 400mL 비커 2 |
| 1 150mL 비커 |
| 1 교반 핫플레이트 |
| 1 교반 막대 |
View the full transcript and gain access to JoVE Lab Manual videos
Q1: What materials do you need to prepare for a borax solubility lab?
Each student pair requires a ring stand, burette clamp, 50-mL glass burette, thermometer clamp, digital and glass thermometers, long-stem funnel, volumetric pipette, pipetter, graduated cylinder, five 250-mL Erlenmeyer flasks, two 400-mL beakers, one 150-mL beaker, and a stirring hotplate with stir bar for heating and mixing solutions.
Q2: How do you prepare a 0.5 M HCl solution for the borax experiment?
Using a volumetric pipette, transfer 20 mL of concentrated HCl to a 500-mL volumetric flask. Dilute the solution to the 500-mL mark with deionized water and mix on a stir plate until homogeneous. Store the prepared solution in an appropriate bottle until the lab session begins.
Q3: Why are different temperatures assigned to lab groups in a solubility experiment?
Assigning each group a specific temperature—10, 20, 30, 40, or 50 °C—allows students to collect solubility data across a temperature range. This approach enables the class to generate a complete solubility curve showing how borax solubility changes with temperature, providing comprehensive experimental data.
Q4: What is the role of bromocresol green indicator in the borax solubility lab?
Bromocresol green indicator is prepared as a 0.1% solution in dropper bottles, one per lab group. It serves as a visual indicator to detect the endpoint during titration, changing color when the acid-base reaction reaches completion, allowing students to accurately determine borax concentration.
Q5: How should you set up the weigh station for borax preparation?
Place a stock bottle of borax, weighing boats, and a spatula at each weigh station. This setup allows students to accurately measure and transfer the required mass of borax for their assigned temperature. Ensure adequate space and organization so multiple groups can weigh samples simultaneously without cross-contamination.
Q6: What is the purpose of using a volumetric pipette in HCl solution preparation?
A volumetric pipette delivers a precise volume of concentrated HCl—exactly 20 mL—ensuring accurate dilution to create a standardized 0.5 M solution. This precision is critical for reproducible experimental results and allows all lab groups to work with identically prepared acid solutions.