Name: Vloeistofcel Raman-spectroscopie voor operando-studies van reactie- en transportverschijnselen tijdens corrosie van silicaatglas (Video) | JoVE Journal
Uploaded: 2025-05-09T13:20:00.000+00:00
Duration: 6 min 48 s
Description: Leer vloeistofcel Raman-spectroscopie toe te passen voor real-time observatie van silicaatglascorrosie bij verhoogde temperaturen. Deze methode biedt inzicht in reactiemechanismen en transportprocessen voor nucleair afvalbeheer.

ai_agent_IP

ai_agent

maintenance

instantTrialDurationMinutes

isBiopharma

enableNewMyJoveSectionDesign

educationFeatures

seoMetaApi

ai_copilot_institution_blacklist

ai_chat_institution_blacklist

freeAccessWindow

ssoRoleCapture

scheduledMaintenanceBanner

joveLabsFeatures

disable_autoplay_for_bots

extended_trial_duration

5 minutes

<ol><li>Belançon, M. P., Sandrini, M., Zanuto, V. S., Muniz, R. F. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Glassy+materials+for+Silicon-based+solar+panels%3A+Present+and+future%5BTitle%5D)+AND+%22J+Non-Crystalline+Solids%22%5BJournal%5D)">Glassy materials for Silicon-based solar panels: Present and future.</a> J Non-Crystalline Solids. 619, 122548(2023).</li>
<li>Iacocca, R., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Factors+affecting+the+chemical+durability+of+glass+used+in+the+pharmaceutical+industry%5BTitle%5D)+AND+%22AAPS+PharmSciTech%22%5BJournal%5D)">Factors affecting the chemical durability of glass used in the pharmaceutical industry.</a> AAPS PharmSciTech. 11 (3), 1340-1349 (2010).</li>
<li>Grambow, B. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((A+general+rate+equation+for+nuclear+waste+glass+corrosion%5BTitle%5D)+AND+%22MRS+Online+Proc+Lib%22%5BJournal%5D)">A general rate equation for nuclear waste glass corrosion.</a> MRS Online Proc Lib. 44, 15-27 (1984).</li>
<li>Gin, S., Taron, M., Arena, H., Delaye, J. M. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Effect+of+structural+disorder+induced+by+external+irradiation+with+heavy+ions+on+the+alteration+of+a+four+oxide+borosilicate+glass%5BTitle%5D)+AND+%22NPJ+Mater+Degrad%22%5BJournal%5D)">Effect of structural disorder induced by external irradiation with heavy ions on the alteration of a four oxide borosilicate glass.</a> NPJ Mater Degrad. 8, 64(2024).</li>
<li>Geisler, T., Dohmen, L., Lenting, C., Fritzsche, M. B. K. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Real-time+in+situ+observations+of+reaction+and+transport+phenomena+during+silicate+glass+corrosion+by+fluid-cell+Raman+spectroscopy%5BTitle%5D)+AND+%22Nat+Mater%22%5BJournal%5D)">Real-time in situ observations of reaction and transport phenomena during silicate glass corrosion by fluid-cell Raman spectroscopy.</a> Nat Mater. 18, 342-348 (2019).</li>
<li>Stroncik, N. A., Schmincke, H. U. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Evolution+of+palagonite%3A+Crystallization%2C+chemical+changes%2C+and+element+budget%5BTitle%5D)+AND+%22Geochem+Geophys+Geosyst%22%5BJournal%5D)">Evolution of palagonite: Crystallization, chemical changes, and element budget.</a> Geochem Geophys Geosyst. 2 (7), 1017(2001).</li>
<li>Staudigel, H., Hart, S. R. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Alteration+of+basaltic+glass%3A+Mechanisms+and+significance+for+the+oceanic+crust-seawater+budget%5BTitle%5D)+AND+%22Geochim+Cosmochim+Acta%22%5BJournal%5D)">Alteration of basaltic glass: Mechanisms and significance for the oceanic crust-seawater budget.</a> Geochim Cosmochim Acta. 47, 337-350 (1983).</li>
<li>Udi, U. J., Yussof, M. M., Ayagi, K. M., Bedon, C., Kamarudin, M. K. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Environmental+degradation+of+structural+glass+systems%3A+A+review+of+experimental+research+and+main+influencing+parameters%5BTitle%5D)+AND+%22Ain+Shams+Eng+J%22%5BJournal%5D)">Environmental degradation of structural glass systems: A review of experimental research and main influencing parameters.</a> Ain Shams Eng J. 14, 101970(2023).</li>
<li>Majérus, O., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Glass+alteration+in+atmospheric+conditions%3A+crossing+perspectives+from+cultural+heritage%2C+glass+industry%2C+and+nuclear+waste+management%5BTitle%5D)+AND+%22NPJMater+Degrad%22%5BJournal%5D)">Glass alteration in atmospheric conditions: crossing perspectives from cultural heritage, glass industry, and nuclear waste management.</a> NPJMater Degrad. 4, 27(2020).</li>
<li>Grambow, B. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Nuclear+waste+glasses+-+How+durable%5BTitle%5D)+AND+%22Elements%22%5BJournal%5D)">Nuclear waste glasses - How durable.</a> Elements. 2, 357-364 (2006).</li>
<li>Hellmann, R., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Nanometre-scale+evidence+for+interfacial+dissolution-reprecipitation+control+of+silicate+glass+corrosion%5BTitle%5D)+AND+%22Nat+Mater%22%5BJournal%5D)">Nanometre-scale evidence for interfacial dissolution-reprecipitation control of silicate glass corrosion.</a> Nat Mater. 14, 307-311 (2015).</li>
<li>Gin, S., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Origin+and+consequences+of+silicate+glass+passivation+by+surface+layers%5BTitle%5D)+AND+%22Nat+Comm%22%5BJournal%5D)">Origin and consequences of silicate glass passivation by surface layers.</a> Nat Comm. 6, 6360-6360 (2015).</li>
<li>Gin, S., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((The+controversial+role+of+inter-diffusion+in+glass+alteration%5BTitle%5D)+AND+%22Chem+Geol%22%5BJournal%5D)">The controversial role of inter-diffusion in glass alteration.</a> Chem Geol. 440, 115-123 (2016).</li>
<li>Gin, S., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((An+international+initiative+on+long-term+behavior+of+high-level+nuclear+waste+glass%5BTitle%5D)+AND+%22Mater+Today%22%5BJournal%5D)">An international initiative on long-term behavior of high-level nuclear waste glass.</a> Mater Today. 16, 243-248 (2013).</li>
<li>Frugier, P., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((SON68+Nuclear+glass+dissolution+kinetics%3A+Current+state+of+knowledge+and+basis+of+the+new+GRAAL+model%5BTitle%5D)+AND+%22J+Nuclear+Mater%22%5BJournal%5D)">SON68 Nuclear glass dissolution kinetics: Current state of knowledge and basis of the new GRAAL model.</a> J Nuclear Mater. 380, 8-21 (2008).</li>
<li>Bunker, B. C. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Molecular+mechanisms+for+corrosion+of+silica+and+silicate+glasses%5BTitle%5D)+AND+%22J+Non-Crystalline+Solids%22%5BJournal%5D)">Molecular mechanisms for corrosion of silica and silicate glasses.</a> J Non-Crystalline Solids. 179, 300-308 (1994).</li>
<li>Cailleteau, C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Insight+into+silicate-glass+corrosion+mechanisms%5BTitle%5D)+AND+%22Nat+Mater%22%5BJournal%5D)">Insight into silicate-glass corrosion mechanisms.</a> Nat Mater. 7, 978-983 (2008).</li>
<li>Gin, S., Ryan, J. V., Schreiber, D. K., Neeway, J., Cabié, M. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Contribution+of+atom-probe+tomography+to+a+better+understanding+of+glass+alteration+mechanisms%3A+Application+to+a+nuclear+glass+specimen+altered+25years+in+a+granitic+environment%5BTitle%5D)+AND+%22Chem+Geol%22%5BJournal%5D)">Contribution of atom-probe tomography to a better understanding of glass alteration mechanisms: Application to a nuclear glass specimen altered 25years in a granitic environment.</a> Chem Geol. 349 - 350, 99-109 (2013).</li>
<li>Geisler, T., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((The+mechanism+of+borosilicate+glass+corrosion+revisited%5BTitle%5D)+AND+%22Geochim+Cosmochim+Acta%22%5BJournal%5D)">The mechanism of borosilicate glass corrosion revisited.</a> Geochim Cosmochim Acta. 158, 112-129 (2015).</li>
<li>Geisler, T., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Aqueous+corrosion+of+borosilicate+glass+under+acidic+conditions%3A+A+new+corrosion+mechanism%5BTitle%5D)+AND+%22J+Non-Crystalline+Solids%22%5BJournal%5D)">Aqueous corrosion of borosilicate glass under acidic conditions: A new corrosion mechanism.</a> J Non-Crystalline Solids. 356, 1458-1465 (2010).</li>
<li>Putnis, A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Why+mineral+interfaces+matter%5BTitle%5D)+AND+%22Science%22%5BJournal%5D)">Why mineral interfaces matter.</a> Science. 343, 1441-1442 (2014).</li>
<li>Putnis, A. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Mineral+replacement+reactions%3A+from+macroscopic+observations+to+microscopic+mechanisms%5BTitle%5D)+AND+%22Mineralogical+Magazine%22%5BJournal%5D)">Mineral replacement reactions: from macroscopic observations to microscopic mechanisms.</a> Mineralogical Magazine. 66, 689-708 (2002).</li>
<li>Lenting, C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Towards+a+unifying+mechanistic+model+for+silicate+glass+corrosion%5BTitle%5D)+AND+%22NPJ+Mater+Degrad%22%5BJournal%5D)">Towards a unifying mechanistic model for silicate glass corrosion.</a> NPJ Mater Degrad. 2, 28(2018).</li>
<li>Fritzsche, M. B. K. <a target="_blank" href="http://scholar.google.com/scholar?hl=en&safe=off&q=%22The+aqueous+corrosion+of+borosilicate+glasses+studied+in+operando+by+in+situ+fluid-cell+Raman+spectroscopy.%22">The aqueous corrosion of borosilicate glasses studied in operando by in situ fluid-cell Raman spectroscopy. Dissertation</a>. , University of Bonn. Germany. https://hdl.handle.net/20.500.11811/10602 (2023).</li>
<li>Iler, K. R. <a target="_blank" href="http://scholar.google.com/scholar?hl=en&safe=off&q=author%3aIler%2C+KR+%22The+chemistry+of+silica%3A+Solubility%2C+polymerization%2C+colloid+and+surface+properties+and+biochemistry+of+silica%22">The chemistry of silica: Solubility, polymerization, colloid and surface properties and biochemistry of silica</a>. , Wiley. (1979).</li>
<li>Gin, S., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((The+fate+of+silicon+during+glass+corrosion+under+alkaline+conditions%3A+A+mechanistic+and+kinetic+study+with+the+International+Simple+Glass%5BTitle%5D)+AND+%22Geochim+Cosmochim+Acta%22%5BJournal%5D)">The fate of silicon during glass corrosion under alkaline conditions: A mechanistic and kinetic study with the International Simple Glass.</a> Geochim Cosmochim Acta. 151, 68-85 (2015).</li>
<li>Putnis, C., Ruiz-Agudo, E. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((The+mineral-water+interface%3A+Where+minerals+react+with+the+environment%5BTitle%5D)+AND+%22Elements%22%5BJournal%5D)">The mineral-water interface: Where minerals react with the environment.</a> Elements. 9, 177-182 (2013).</li>
<li>Icenhower, J. P., Steefel, C. I. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Dissolution+rate+of+borosilicate+glass+SON68%3A+A+method+of+quantification+based+upon+interferometry+and+implications+for+experimental+and+natural+weathering+rates+of+glass%5BTitle%5D)+AND+%22Geochim+Cosmochim+Acta%22%5BJournal%5D)">Dissolution rate of borosilicate glass SON68: A method of quantification based upon interferometry and implications for experimental and natural weathering rates of glass.</a> Geochim Cosmochim Acta. 157, 147-163 (2015).</li>
<li>Icenhower, J. P., Steefel, C. I. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Experimentally+determined+dissolution+kinetics+of+SON68+glass+at+90%C2%B0C+over+a+silica+saturation+interval%3A+Evidence+against+a+linear+rate+law%5BTitle%5D)+AND+%22J+Nuc+Mater%22%5BJournal%5D)">Experimentally determined dissolution kinetics of SON68 glass at 90°C over a silica saturation interval: Evidence against a linear rate law.</a> J Nuc Mater. 439, 137-147 (2013).</li>
<li>Lenting, C., Geisler, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Corrosion+of+ternary+borosilicate+glass+in+acidic+solution+studied+in+operando+by+fluid-cell+Raman+spectroscopy%5BTitle%5D)+AND+%22NPJ+Mater+Degrad%22%5BJournal%5D)">Corrosion of ternary borosilicate glass in acidic solution studied in operando by fluid-cell Raman spectroscopy.</a> NPJ Mater Degrad. 5, 37(2021).</li>
<li>Lönartz, M. I., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((The+effect+of+heavy+ion+irradiation+on+the+forward+dissolution+rate+of+borosilicate+glasses+studied+in+situ+and+real+time+by+fluid-cell+raman+spectroscopy%5BTitle%5D)+AND+%22Materials%22%5BJournal%5D)">The effect of heavy ion irradiation on the forward dissolution rate of borosilicate glasses studied in situ and real time by fluid-cell raman spectroscopy.</a> Materials. 12 (9), 1480(2019).</li>
<li>Müller, G., Fritzsche, M. B. K., Dohmen, L., Geisler, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Feedbacks+and+non-linearity+of+silicate+glass+alteration+in+hyperalkaline+solution+studied+by+in+operando+fluid-cell+Raman+spectroscopy%5BTitle%5D)+AND+%22Geochim+Cosmochim+Acta%22%5BJournal%5D)">Feedbacks and non-linearity of silicate glass alteration in hyperalkaline solution studied by in operando fluid-cell Raman spectroscopy.</a> Geochim Cosmochim Acta. 329, 1-21 (2022).</li>
<li>Müller, G. <a target="_blank" href="http://scholar.google.com/scholar?hl=en&safe=off&q=author%3aM%C3%BCller%2C+G+%22Raman+spectroscopic+ex+situ+and+in+situ.+investigations+of+the+aqueous+corrosion+of+soda-lime+silicate+glasses%22">Raman spectroscopic ex situ and in situ. investigations of the aqueous corrosion of soda-lime silicate glasses</a>. , University of Bonn. Bonn. (2019).</li>
<li>Sulzbach, M., Geisler, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((The+replacement+of+celestine+%28SrSO4%29+by+strontianite+%28SrCO3%29+in+aqueous+solution+studied+in+situ+and+in+real+time+using+fluid-cell+Raman+spectroscopy%5BTitle%5D)+AND+%22Minerals%22%5BJournal%5D)">The replacement of celestine (SrSO4) by strontianite (SrCO3) in aqueous solution studied in situ and in real time using fluid-cell Raman spectroscopy.</a> Minerals. 14 (2), 164(2024).</li>
<li>Dohmen, L. <a target="_blank" href="http://scholar.google.com/scholar?hl=en&safe=off&q=%22In+situ+.observations+of+reaction+and+transport+phenomena+during+silicate+glass+corrosion+by+fluid-cell+Raman+spectroscopy%3A+Method+development+and+applications.+Unpubl.%22">In situ .observations of reaction and transport phenomena during silicate glass corrosion by fluid-cell Raman spectroscopy: Method development and applications. Unpubl. PhD thesis</a>. , University of Bonn. Germany. (2019).</li>
<li>Everall, N. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Confocal+Raman+microscopy%3A+Why+the+depth+resolution+and+spatial+accuracy+can+be+much+worse+than+you+think%5BTitle%5D)+AND+%22Appl+Spectrosc%22%5BJournal%5D)">Confocal Raman microscopy: Why the depth resolution and spatial accuracy can be much worse than you think.</a> Appl Spectrosc. 54, 1515-1520 (2000).</li>
<li>Everall, N. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Depth+profiling+with+confocal+raman+microscopy%2C+part+II%5BTitle%5D)+AND+%22Spectroscopy%22%5BJournal%5D)">Depth profiling with confocal raman microscopy, part II.</a> Spectroscopy. 19, 22-27 (2004).</li>
<li>Everall, N. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((The+influence+of+out-of-focus+sample+regions+on+the+surface+specificity+of+confocal+Raman+microscopy%5BTitle%5D)+AND+%22Appl+Spectrosc%22%5BJournal%5D)">The influence of out-of-focus sample regions on the surface specificity of confocal Raman microscopy.</a> Appl Spectrosc. 62, 591-598 (2008).</li>
<li>Hauke, K., Kehren, J., Böhme, N., Zimmer, S., Geisler-Wierwille, T. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((In+situ+hyperspectral+Raman+Imaging%3A+A+new+method+to+investigate+sintering+processes+of+ceramic+material+at+high-temperature%5BTitle%5D)+AND+%22Appl+Sci%22%5BJournal%5D)">In situ hyperspectral Raman Imaging: A new method to investigate sintering processes of ceramic material at high-temperature.</a> Appl Sci. 9, 1310(2019).</li>
<li>Davis, K. M., Tomozawa, M. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((An+infrared+spectroscopic+study+of+water-related+species+in+silica+glasses%5BTitle%5D)+AND+%22J+Non-Crystalline+Solids%22%5BJournal%5D)">An infrared spectroscopic study of water-related species in silica glasses.</a> J Non-Crystalline Solids. 201, 177-198 (1996).</li>
<li>Long, D. A. <a target="_blank" href="http://scholar.google.com/scholar?hl=en&safe=off&q=author%3aLong%2C+DA+%22Raman+spectroscopy%22">Raman spectroscopy</a>. , McGraw Hill International Book Company. Great Britain. (1977).</li>
</ol>

<table><tbody><tr><td>Schroefdraadverbindingen (6 stuks)</td><td>---</td><td>---</td><td></td></tr><tr><td>Blauw siliconen draad</td><td>Reichelt Elektronik</td><td></td><td>doorsnede:&nbsp; 1,5 mm&sup2;, lengte: 2 m</td></tr><tr><td>Condensator</td><td>Reichelt Elektronik</td><td></td><td>capaciteit: 100 nF</td></tr><tr><td>Aansluitingen naar keuze van de gebruiker&lsquo;s</td><td>Reichelt Elektronik</td><td></td><td></td></tr><tr><td>Eurotherm Controller 3216</td><td>Eurotherm/Emerson</td><td>Bestelcode 3216 CC VH LXXX X XXX G ENG XXXXX</td><td></td></tr><tr><td>Flensloze ferrules ETFE&nbsp;</td><td>Darwin Microfluidics</td><td>SKU: ID-P-200X</td><td>1/4"-28 voor 1/16" OD&nbsp;</td></tr><tr><td>Vloeistofcel (container + deksel)</td><td>zelfgemaakt</td><td>---</td><td>technische tekening is opgenomen in de bijlage (S1-S2)</td></tr><tr><td>Verwarmingselement, metaal-keramisch verwarmingselement (MCH) schijf</td><td>Alibaba</td><td></td><td>D: 30 mm, H: 1,5 mm; https://german.alibaba.com/product-detail/DC-Power-Supply-30mm-MCH-Round-1600118228465.html?spm=a 2700.7724857.0.0.7cde5nqq5nqq2n</td></tr><tr><td>Horiba HR800 Raman spectrometer</td><td>HORIBA</td><td></td><td></td></tr><tr><td>LabSpec 6.5.1.24 Spectroscopy Suite</td><td></td><td></td><td></td></tr><tr><td>Netsnoer met stekker, belasting+neutraal (L+N)</td><td>Reichelt Elektronik</td><td></td><td>lengte: 2 m</td></tr><tr><td>Netzekering 1A&nbsp;</td><td>Reichelt Elektronik</td><td></td><td>5x20 mm&sup2;</td></tr><tr><td>Netzekeringhouder&nbsp;</td><td>Reichelt Elektronik</td><td></td><td>5x20 mm&sup2;</td></tr><tr><td>Netschakelaar&nbsp;</td><td>Reichelt Elektronik</td><td></td><td>230VAC 2A</td></tr><tr><td>Microfluidische aansluitingen Adapter Female Luer naar 1/4-28 Male&nbsp;</td><td>Darwin Microfluidics</td><td>SKU: ID-P-618</td><td></td></tr><tr><td>Millex Spuitfilters</td><td>Merck</td><td>SLGPR33RS</td><td></td></tr><tr><td>NaHCO3</td><td>Merck</td><td>CAS-144-55-8</td><td></td></tr><tr><td>NMOS Mosfet F1010N</td><td>Reichelt Elektronik</td><td></td><td></td></tr><tr><td>Kunststof behuizing</td><td>Reichelt Elektronik</td><td>TEKO KL22</td><td>Behuizing 178x128x72</td></tr><tr><td>PTFE monsterhouder</td><td>zelfgemaakt</td><td>---</td><td></td></tr><tr><td>PTFE slang&nbsp;</td><td>Darwin Microfluidics</td><td>BL-PTFE-1608-20</td><td>1/16" OD</td></tr><tr><td>Rode siliconen draad</td><td>Reichelt Elektronik</td><td></td><td>doorsnede: 1,5 mm&sup2;, lengte: 2 m</td></tr><tr><td>Weerstand</td><td>Reichelt Elektronik</td><td></td><td>1/4W, 10kOhm</td></tr><tr><td>Weerstand</td><td>Reichelt Elektronik</td><td></td><td>1/4W, 2,2kOhm</td></tr><tr><td>Saffiervenster&nbsp;</td><td>Edmund Optics GmbH</td><td>#71-225</td><td>D: 15 mm H: 100 &micro;m</td></tr><tr><td>Afsluitventiel 1/4-28&nbsp;</td><td>Darwin Microfluidics</td><td>SKU: ID-P-782&nbsp;</td><td></td></tr><tr><td>Siliconen ring</td><td>ART Elektromechanik</td><td>aangepast voor instituut</td><td>OD: 15mm, ID: 8 mm; H: 0,5 mm</td></tr><tr><td>Schakelvermogen&nbsp;</td><td>Reichelt Elektronik</td><td>SNT RS 25 5</td><td>5V, 5A</td></tr><tr><td>Thermokoppelverlengkabel, stekker/stopcontact, type K</td><td>RS Components GmbH</td><td></td><td>2 m</td></tr><tr><td>Thermokoppelstopcontact, type K, behuizingsmontage</td><td>RS Components GmbH</td><td></td><td></td></tr><tr><td>Thermokoppel, type K</td><td>TC Direct</td><td></td><td>D: 1 mm, L: 50-100mm</td></tr><tr><td>Verschillende kabels voor bedrading in de doos</td><td>Reichelt Elektronik</td><td></td><td></td></tr></tbody></table>

vloeistofcel raman-spectroscopie voor operando-studies van reactie- en transportverschijnselen tijdens corrosie van silicaatglas

Fluid-cell Raman Spectroscopy for operando Studies of Reaction and Transport Phenomena during Silicate Glass Corrosion

Vloeistofcel Raman-spectroscopie voor operando-studies van reactie- en transportverschijnselen tijdens corrosie van silicaatglas

Fluid-cell Raman Spectroscopy (FCRS) enables the real-time and space-resolved (operando) study of reaction mechanisms, kinetics, and their mutual ...

fluid-cell-raman-spectroscopy-for-operando-studies-reaction-transport

Research

JoVE Journal

Chemistry

Scheikunde

We bespreken de bouw en exploitatie van een complex niet-lineaire optische systeem dat ultrasnelle all-optisch schakelen gebruikt om te isoleren Raman van fluorescentie-signalen. Met behulp van dit systeem zijn wij in staat om succesvol scheiden Raman en fluorescentie-signalen gebruik te maken van puls energie en de gemiddelde krachten die blijven biologisch veilig.

Verwerping van Fluorescentie Achtergrond in Resonance en spontane Raman Microspectroscopie

Raman spectroscopie is een geschikte techniek voor de non-contact, label-free analyse van levende cellen, weefsel-engineering constructen en cellen. Bronspecifieke spectrale vingerafdrukken worden gegenereerd en geanalyseerd met multivariate analyse.

Non-contact, Label-free monitoring van cellen en extracellulaire matrix met behulp van Raman spectroscopie

We hebben een self-contained vloeibare cel die imaging doorlaat vloeistoffen met een transmissie-elektronenmicroscoop. Dynamische processen van nanodeeltjes in vloeistoffen kan worden onthuld in real-time met sub-nanometer resolutie.

Onthulling dynamische processen van de grondstoffen in vloeistoffen met behulp van vloeibare Cell Transmissie Elektronen Microscopie

We presenteren een uniek platform voor het karakteriseren van elektrode oppervlakken in vaste oxide brandstofcel (SOFC) die gelijktijdig uitvoeren van meerdere karakterisatietechnieken...

Indringende en in kaart brengen van elektrode-oppervlakken in Solid Oxide Fuel Cells

Real-time monitoring zorgt voor een snelle optimalisatie van de reacties uitgevoerd met behulp van een continue flow verwerking. Hier is de bereiding van 3-acetylcumarine wordt als voorbeeld gebruikt. De inrichting voor het uitvoeren van in situ-Raman bewaking wordt beschreven, evenals de stappen die nodig zijn om de reactie te optimaliseren.

Real-time monitoring van de reacties uitgevoerd met behulp van continue flow Verwerking: De Bereiding van 3-acetylcumarine als een voorbeeld

Hier presenteren we een protocol voor afkoelsnelheid afhankelijke ellipsometrie experimenten, waarbij de glasovergangstemperatuur (Tg) kan bepalen, gemiddeld dynamiek, kwetsbaarheid en de uitzettingscoëfficiënt van de onderkoelde vloeistof en glas voor een verscheidenheid van glasachtige materialen.

Koeling Rate Afhankelijk Ellipsometrie Metingen aan de dynamiek van Thin Films glazige Bepaal

Een protocol voor stapsgewijze Raman en IR spectroelectrochemical analyse wordt gepresenteerd.

Raman en IR Spectroelectrochemical methoden als hulpmiddelen voor het analyseren van geconjugeerd organische stoffen

Hier presenteren we een protocol om te beschrijven van ex situ en in situ onderzoeken van structurele transformaties in metalen bril. Wij dienst nucleaire gebaseerde analysemethoden die hyperfine interacties keuren. We tonen de toepasselijkheid van Mössbauer spectrometrie en nucleaire voorwaartse verstrooiing van synchrotronstraling tijdens temperatuur gestuurde experimenten.

Methoden van Ex Situ en In Situ onderzoeken van structurele transformaties: het geval van kristallisatie van metalen bril

Het gebruik van FTIR spectroscopie voor onderzoek naar de oppervlakte-eigenschappen van polykristallijne vaste stoffen wordt beschreven. De voorbereiding van monsterpellets, activeringsprocedures, karakterisering met sondemoleculen en modelstudies van CO 2-adsorptie worden besproken.

In situ FTIR Spectroscopie als hulpmiddel voor onderzoek naar gas/vaste interactie: waterversterkte CO2 Adsorptie in UiO-66 Metaal-Organisch Framework

Dit protocol presenteert een geïntegreerde Ramanspectroscopie-massaspectrometrie (MS) platform dat is geschikt voor het bereiken van één-cel resolutie. Raman-spectroscopie kan worden gebruikt om cellulaire reactie op drugs te bestuderen, terwijl MS kan worden gebruikt voor gerichte en kwantitatieve analyse van de opname van geneesmiddelen en metabolisme.

Een geïntegreerde Raman-spectroscopie en massaspectrometrie platform voor het bestuderen van de opname van één cel drug, metabolisme, en effecten

Hier presenteren we een protocol voor het uitvoeren van TEM-gasreactie-experimenten met gesloten cellen in situ, terwijl we verschillende veelgebruikte monstervoorbereidingsmethoden beschrijven.

In situ gesloten-cel gasreacties uitvoeren in de transmissie-elektronenmicroscoop

Leer vloeistofcel Raman-spectroscopie toe te passen voor real-time observatie van silicaatglascorrosie bij verhoogde temperaturen. Deze methode biedt inzicht in reactiemechanismen en transportprocessen voor nucleair afvalbeheer.

Vloeistofcel Raman-spectroscopie voor operando-studies van reactie- en transportverschijnselen tijdens corrosie van silicaatglas (Video) | JoVE Journal

Vloeistofcel Raman-spectroscopie voor operando-studies van reactie- en transportverschijnselen tijdens corrosie van silicaatglas

Meer video's verkennen