Name: Synthese en prestatie-evaluaties van ZnCoS/ZnCdS met dubbele kristalstructuur voor multifunctionele redox-fotokatalyse in energietoepassingen (Video) | JoVE Journal
Uploaded: 2025-07-25T14:45:00.000+00:00
Duration: 9 min 22 s
Description: Ontdek de synthese van ZnCoS/ZnCdS-fotokatalysatoren met dubbele kristalstructuur voor waterstofproductie en benzaldehyde-synthese. Deze methode verbetert zichtbaarlichtabsorptie en ladingscheiding voor duurzame energieconversie.

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<ol><li>Wong, K. J., Foo, J. J., Siang, T. J., Ong, W. J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Shining+light+on+carbon+aerogel+photocatalysts%3A+Unlocking+the+potentials+in+the+quest+for+revolutionizing+solar-to-chemical+conversion+and+environmental+remediation%5BTitle%5D)+AND+%22Adv+Funct+Mater%22%5BJournal%5D)">Shining light on carbon aerogel photocatalysts: Unlocking the potentials in the quest for revolutionizing solar-to-chemical conversion and environmental remediation.</a> Adv Funct Mater. 33 (50), 2306014(2023).</li>
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<li>Meng, S., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Efficient+photocatalytic+H2+evolution%2C+CO2+reduction+and+N2+fixation+coupled+with+organic+synthesis+by+co-catalyst+and+vacancies+engineering%5BTitle%5D)+AND+%22Appl+Catal+B+Environ%22%5BJournal%5D)">Efficient photocatalytic H2 evolution, CO2 reduction and N2 fixation coupled with organic synthesis by co-catalyst and vacancies engineering.</a> Appl Catal B Environ. 285, 119789(2021).</li>
<li>Lei, J., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Optimization+of+adsorption+sites+for+selective+hydrobenzoin+and+syngas+production+in+a+single+photoredox+cycle%5BTitle%5D)+AND+%22Adv+Energy+Mater%22%5BJournal%5D)">Optimization of adsorption sites for selective hydrobenzoin and syngas production in a single photoredox cycle.</a> Adv Energy Mater. 15, 2500950(2025).</li>
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<li>Su, B. J., Foo, J. J., Ling, G. Z. S., Ong, W. J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Ternary+heterojunctions+on+Zn3In2S6%2FC3N5+towards+advancing+simultaneous+photocatalytic+production+of+H2O2+and+benzaldehyde%5BTitle%5D)+AND+%22Green+Chem+Eng%22%5BJournal%5D)">Ternary heterojunctions on Zn3In2S6/C3N5 towards advancing simultaneous photocatalytic production of H2O2 and benzaldehyde.</a> Green Chem Eng. , (2025).</li>
<li>Khoo, V., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Carbon+doping+in+crystalline+C3N5+photocatalyst%3A+Unraveling+CH+functional+groups+for+near-unity+electron-hole+utilization+toward+ameliorated+dual-functional+H2O2+and+benzaldehyde+co-production%5BTitle%5D)+AND+%22Appl+Catal+B+Environ+Energy%22%5BJournal%5D)">Carbon doping in crystalline C3N5 photocatalyst: Unraveling CH functional groups for near-unity electron-hole utilization toward ameliorated dual-functional H2O2 and benzaldehyde co-production.</a> Appl Catal B Environ Energy. 372, 125294(2025).</li>
<li>Tan, X. Q., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Elevating+dual-redox+photocatalysis+with+p-n+junction%3A+Hydrangea-like+Zn3In2S6+nanoflowers+coupled+hexagonal+Co3O4+for+cooperative+hydrogen+and+benzaldehyde+production%5BTitle%5D)+AND+%22Nano+Mater+Sci%22%5BJournal%5D)">Elevating dual-redox photocatalysis with p-n junction: Hydrangea-like Zn3In2S6 nanoflowers coupled hexagonal Co3O4 for cooperative hydrogen and benzaldehyde production.</a> Nano Mater Sci. 7 (2), 169-179 (2025).</li>
<li>Foo, J. J., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Synergistic+potassium+intercalation+and+cyano+group+modification+on+crystalline+carbon+nitride+homojunction+towards+dual-functional+photoredox+coupling+of+H2O2+and+benzaldehyde+production%5BTitle%5D)+AND+%22Chem+Eng+J%22%5BJournal%5D)">Synergistic potassium intercalation and cyano group modification on crystalline carbon nitride homojunction towards dual-functional photoredox coupling of H2O2 and benzaldehyde production.</a> Chem Eng J. 505, 158992(2025).</li>
<li>Fang, B., Xing, Z., Sun, D., Li, Z., Zhou, W. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Hollow+semiconductor+photocatalysts+for+solar+energy+conversion%5BTitle%5D)+AND+%22Adv+Powder+Mater%22%5BJournal%5D)">Hollow semiconductor photocatalysts for solar energy conversion.</a> Adv Powder Mater. 1 (2), 100021(2022).</li>
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<li>Du, H., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Bare+Cd1-xZnxS+ZB%2FWZ+heterophase+nanojunctions+for+visible+light+photocatalytic+hydrogen+production+with+high+efficiency%5BTitle%5D)+AND+%22ACS+Appl+Mater+Interfaces%22%5BJournal%5D)">Bare Cd1-xZnxS ZB/WZ heterophase nanojunctions for visible light photocatalytic hydrogen production with high efficiency.</a> ACS Appl Mater Interfaces. 8 (37), 24550-24558 (2016).</li>
<li>Zhao, H., Zhao, X., Shen, L., Liu, H., Li, X. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Synergistic+effects+of+co-catalyst+and+homojunction%2Fheterojunction+with+boosted+photocatalytic+H2+evolution+over+Zn0.5Cd0.5S%2FNDs%5BTitle%5D)+AND+%22Chem+Eng+J%22%5BJournal%5D)">Synergistic effects of co-catalyst and homojunction/heterojunction with boosted photocatalytic H2 evolution over Zn0.5Cd0.5S/NDs.</a> Chem Eng J. 470, 143925(2023).</li>
<li>Dong, J., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Few-layered+MoS2%2FZnCdS%2FZnS+heterostructures+with+an+enhanced+photocatalytic+hydrogen+evolution%5BTitle%5D)+AND+%22ACS+Appl+Mater+Interfaces%22%5BJournal%5D)">Few-layered MoS2/ZnCdS/ZnS heterostructures with an enhanced photocatalytic hydrogen evolution.</a> ACS Appl Mater Interfaces. 5 (4), 4893-4902 (2022).</li>
<li>Liu, Y., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Recent+advances+in+the+hydrogen+evolution+reaction+of+ZnxCd1-xS-based+photocatalysts%5BTitle%5D)+AND+%22Solar+RRL%22%5BJournal%5D)">Recent advances in the hydrogen evolution reaction of ZnxCd1-xS-based photocatalysts.</a> Solar RRL. 6 (4), 2101061(2022).</li>
<li>Song, Y., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Heterojunction+engineering+of+multinary+metal+sulfide-based+photocatalysts+for+efficient+photocatalytic+hydrogen+evolution%5BTitle%5D)+AND+%22Adv+Mater%22%5BJournal%5D)">Heterojunction engineering of multinary metal sulfide-based photocatalysts for efficient photocatalytic hydrogen evolution.</a> Adv Mater. 36 (11), 2305835(2024).</li>
<li>Chen, H. C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Metal-organic+framework-assisted+synthesis+of+three-dimensional+ZnCoS+effloresced+nanopillars%40CNT+paper+for+high-performance+flexible+all-solid-state+battery-type+supercapacitors+with+ultrahigh+specific+capacitance%5BTitle%5D)+AND+%22ACS+Appl+Energy+Mater%22%5BJournal%5D)">Metal-organic framework-assisted synthesis of three-dimensional ZnCoS effloresced nanopillars@CNT paper for high-performance flexible all-solid-state battery-type supercapacitors with ultrahigh specific capacitance.</a> ACS Appl Energy Mater. 5 (7), 8262-8272 (2022).</li>
<li>Gautam, J., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Fabrication+of+polyoxometalate+anchored+zinc+cobalt+sulfide+nanowires+as+a+remarkable+bifunctional+electrocatalyst+for+overall+water+splitting%5BTitle%5D)+AND+%22Adv+Funct+Mater%22%5BJournal%5D)">Fabrication of polyoxometalate anchored zinc cobalt sulfide nanowires as a remarkable bifunctional electrocatalyst for overall water splitting.</a> Adv Funct Mater. 31 (46), 2106147(2021).</li>
<li>Chen, P., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Distinctive+formation+of+bifunctional+ZnCoS-rGO+3D+hollow+microsphere+flowers+with+excellent+energy+storage+performances%5BTitle%5D)+AND+%22Chem+Mater%22%5BJournal%5D)">Distinctive formation of bifunctional ZnCoS-rGO 3D hollow microsphere flowers with excellent energy storage performances.</a> Chem Mater. 34 (13), 5896-5611 (2022).</li>
<li>Siang, T. J., Zhang, P., Chen, B., Ong, W. J. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Surface+defect+engineering+of+ZnCoS+in+ZnCdS+with+twin+crystal+structure+for+visible-light-driven+H2+production+coupled+with+benzyl+alcohol+oxidation%5BTitle%5D)+AND+%22Chin+J+Catal%22%5BJournal%5D)">Surface defect engineering of ZnCoS in ZnCdS with twin crystal structure for visible-light-driven H2 production coupled with benzyl alcohol oxidation.</a> Chin J Catal. 69 (2), 84-98 (2025).</li>
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<li>Wang, J., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Synergistic+promotion+effect+of+ZnCoS+solid+solution+and+Co1-xS+on+photocatalytic+hydrogen+production+of+the+CdS+composite%5BTitle%5D)+AND+%22Langmuir%22%5BJournal%5D)">Synergistic promotion effect of ZnCoS solid solution and Co1-xS on photocatalytic hydrogen production of the CdS composite.</a> Langmuir. 37 (43), 12654-12662 (2021).</li>
<li>Li, C., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((ZnCo2S4%2FZn0.2Cd0.8S+Z-scheme+heterojunction%3A+Efficient+photocatalytic+H2+evolution+coupling+selective+oxidation+of+benzyl+alcohol%5BTitle%5D)+AND+%22Int+J+Hydrogen+Energy%22%5BJournal%5D)">ZnCo2S4/Zn0.2Cd0.8S Z-scheme heterojunction: Efficient photocatalytic H2 evolution coupling selective oxidation of benzyl alcohol.</a> Int J Hydrogen Energy. 47 (92), 38951-38963 (2022).</li>
<li>Mao, Q., et al. <a target="_blank" href="http://www.ncbi.nlm.nih.gov/pubmed?term=((Few-layered+1T-MoS2-modified+ZnCoS+solid-solution+hollow+dodecahedra+for+enhanced+photocatalytic+hydrogen+evolution%5BTitle%5D)+AND+%22J+Mater+Chem+A%22%5BJournal%5D)">Few-layered 1T-MoS2-modified ZnCoS solid-solution hollow dodecahedra for enhanced photocatalytic hydrogen evolution.</a> J Mater Chem A. 7 (14), 8472-8484 (2019).</li>
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</ol>

```html
<table><tbody><tr><td>Benzyl alcohol</td><td>Sigma-Aldrich</td><td>402834</td><td>ACS reagent grade, &ge; 99.0%</td></tr><tr><td>Cadmium acetate dihydrate (Cd(CH3COO)2&middot;2H2O)</td><td>Sigma-Aldrich</td><td>289159</td><td>Reagent grade, 98%</td></tr><tr><td>Cobalt(II) acetate tetrahydrate (Co(CH3COO)2&middot;4H2O)</td><td>Sigma-Aldrich</td><td>403024</td><td>ACS reagent, &ge; 98.0%</td></tr><tr><td>Ethylene glycol</td><td>Sigma-Aldrich</td><td>102466</td><td>ReagentPlus, &ge; 99%</td></tr><tr><td>Gas chromatography</td><td>Agilent</td><td>8890 GC System</td><td>Aangepast, bestaat uit vlamionisatiedetector (FID), thermische geleidbaarheidsdetector (TCD), methanizer, twee MolSieve 5A 60/80 mesh kolommen en drie HayeSep Q 80/100 mesh kolommen</td></tr><tr><td>High-performance liquid chromatography</td><td>Agilent</td><td>1260 Infinity II LC System</td><td>Bestaat uit fotodiode array detector (PAD) en Kinetex 2.6 &mu;m Fenyl-Hexyl 100 &Aring; kolom</td></tr><tr><td>High-speed centrifuge&nbsp;</td><td>Thermo Fisher Scientific</td><td>75009760</td><td>Sorvall X1R Pro</td></tr><tr><td>Magnetic stirrer&nbsp;</td><td>IKA</td><td>3622000</td><td>RET basic</td></tr><tr><td>Mass flow controller</td><td>Alicat</td><td>MC series</td><td></td></tr><tr><td>Nitrogen</td><td>Air Liquide</td><td></td><td>99.9995% zuiverheid</td></tr><tr><td>Oven</td><td>Memmert</td><td>MMT-UN55</td><td></td></tr><tr><td>Sodium sulfide hydrate (Na2S&middot;xH2O)</td><td>Sigma-Aldrich</td><td>13468</td><td>&ge;60%, schalen</td></tr><tr><td>Thioacetamide (CH3CSNH2)</td><td>Sigma-Aldrich</td><td>163678</td><td>ACS reagent grade, &ge; 99.0%, solid</td></tr><tr><td>Three-necked top-irradiation glass reactor&nbsp;</td><td>PTL Glass Aluminium&nbsp;</td><td>Aangepast</td><td></td></tr><tr><td>Ultrasonicator bath</td><td>Cole-Parmer</td><td>CP/P-08895-15</td><td></td></tr><tr><td>Xenon lamp</td><td>Beijing China Education Au-light</td><td>CEL-PF300-T6</td><td></td></tr><tr><td>Zinc acetate dihydrate (Zn(CH3COO)2&middot;2H2O)</td><td>Sigma-Aldrich</td><td>383058</td><td>ACS reagent, &ge; 98.0%</td></tr></tbody></table>
```

synthese en prestatie-evaluaties van zncos/zncds met dubbele kristalstructuur voor multifunctionele redox-fotokatalyse in energietoepassingen

Synthesis and Performance Evaluations of ZnCoS/ZnCdS with Twin Crystal Structure for Multifunctional Redox Photocatalysis in Energy Applications

Synthese en prestatie-evaluaties van ZnCoS/ZnCdS met dubbele kristalstructuur voor multifunctionele redox-fotokatalyse in energietoepassingen

This protocol presents both the synthesis of the visible-light-responsive ZnCoS/ZnCdS with twin crystal structure photocatalyst and the photoredox ...

synthesis-performance-evaluations-zncoszncds-with-twin-crystal

Research

JoVE Journal

Chemistry

Scheikunde

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Fotochemische oxidatieve groei van Iridium Oxide Nanodeeltjes op CdSe @ CdS nanorods

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Ontdek de synthese van ZnCoS/ZnCdS-fotokatalysatoren met dubbele kristalstructuur voor waterstofproductie en benzaldehyde-synthese. Deze methode verbetert zichtbaarlichtabsorptie en ladingscheiding voor duurzame energieconversie.

Synthese en prestatie-evaluaties van ZnCoS/ZnCdS met dubbele kristalstructuur voor multifunctionele redox-fotokatalyse in energietoepassingen (Video) | JoVE Journal

Synthese en prestatie-evaluaties van ZnCoS/ZnCdS met dubbele kristalstructuur voor multifunctionele redox-fotokatalyse in energietoepassingen

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