go to jove.com

HIGH SCHOOL

Chemistry

Concept Videos

Analytical Chemistry

This is a free preview. For full access

Atomic Spectroscopy

AAS Sample Prep and Calibration

Description

Atomic absorption spectroscopy (AAS) depends on careful sample preparation and calibration. Samples must be turned into clear solutions before measurement. That often means extra treatment to dissolve materials such as soils, animal tissues, and minerals.

Common sample prep methods include hot mi...

Transcript

In atomic absorption measurements, solid samples are dissolved in a suitable solvent to form a clear solution before atomization.

Insoluble samples are digested with hot mineral acids, either on a hot plate or through microwave heating.

Other methods to obtain clear solutions include oxidizing the sample with liquid reagents, combu...

Tags

Sample PreparationFlame AtomizationElectrothermal AtomizationCalibration CurvesStandard Addition MethodDetection LimitsNebulizer EfficiencyChelate ExtractionAnalytical Methods