Unknown Gas Identification

Unknown gas identification is the analytical process of determining the composition or identity of a gaseous sample by examining its physical and chemical properties. In chemistry, investigators collect the gas safely and apply characteristic tests, such as observing whether it relights a glowing splint, produces a pop with a flame, turns limewater milky, or changes indicator color. These reactions reflect specific properties of gases including oxidizing behavior, combustibility, acid-base chemistry, and reaction with aqueous solutions. The approach supports laboratory analysis, environmental monitoring, industrial quality control, and practical instruction in chemical observation, while careful controls and multiple tests improve confidence in the result.

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JoVE Lab Manual - Chemistry

Identification of Unknown Aldehydes and Ketones - Student Protocol

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2020

Source: Lara Al Hariri and Ahmed Basabrain at the University of Massachusetts Amherst, MA, USA DNPH Test for Aromatic Aldehydes and KetonesExpand In this lab, you'll use the DNPH test, the Tollens' test, and the iodoform test to identify two unknown aldehydes or ketones. You'll use butanone and benzaldehyde as known compounds to confirm that the tests are working as expected. You'll start the lab with the DNPH test, which relies on the reaction between 2,4-dinitrophenylhydrazine, or DNPH,...

Identification of Unknown Aldehydes and Ketones - Instructor Prep

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2020

Source: Lara Al Hariri at the University of Massachusetts Amherst, MA, USA Preparation of Test SolutionsExpand Here, we show the laboratory preparation for 10 students working in pairs, with some excess. Please adjust quantities as needed. Before you start, put on a lab coat, splash-proof safety glasses, and nitrile gloves. Note: DNPH is a shock explosive, so handle it gently with low friction tools. Phosphoric acid is also toxic and corrosive. Prepare 100 mL of a 0.1 M...

Identification of Unknown Aldehydes and Ketones - Concepts

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2020

Aldehydes and Ketones Aldehydes and ketones have a carbonyl group (C=O) as a functional group. A ketone has two alkyl or aryl groups attached to the carbonyl carbon (RCOR’). The simplest ketone is acetone, which has two methyl groups attached to the carbonyl carbon (CH3COCH3). An aldehyde is similar to a ketone, except that instead of two side groups connected to the carbonyl carbon, they have at least one hydrogen (RCOH). The simplest aldehyde is formaldehyde (HCOH), as it has two hydrogens...

Ideal Gas Law - Student Protocol

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2020

Source: Smaa Koraym at Johns Hopkins University, MD, USA Determining the Mass of the Unknown LiquidExpand According to the ideal gas law for a given pressure, temperature, and volume, the number of moles of gas in that volume is always the same. In this lab, you will use that relationship to calculate the molar mass of an unknown liquid. You will immerse a Dumas tube containing the unknown liquid in boiling water to vaporize the solvent. After waiting a few minutes for the vapor to...

Freezing-Point Depression to Determine an Unknown Compound

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2023

Source: Laboratory of Lynne O' Connell — Boston College When a solid compound is dissolved in a solvent, the freezing point of the resulting solution is lower than that of the pure solvent. This phenomenon is known as freezing-point depression, and the change in temperature is directly related to the molecular weight of the solute. This experiment is designed to find the identity of an unknown compound by using the phenomenon of freezing-point depression to determine its molecular weight. The...

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