Zeolite Synthesis

Zeolite synthesis is the controlled production of crystalline, microporous materials whose interconnected channels and cages can selectively adsorb molecules and exchange ions. It typically involves dissolving or aging aluminosilicate precursors with a mineralizing agent and, often, an organic structure-directing agent, followed by hydrothermal or solvothermal crystallization, washing, drying, and activation. Adjusting composition, pH, temperature, time, and template chemistry determines the zeolite’s framework, pore size, acidity, and particle properties. In neuroscience-related research, these tunable materials can support molecular separations, biosensing, adsorption of metabolites or toxins, and controlled delivery strategies, making synthesis conditions important for developing reproducible tools for brain research.

Zeolite Synthesis - Related Videos

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JoVE Journal - Chemistry
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Synthesis of Zeolites Using the ADOR (Assembly-Disassembly-Organization-Reassembly) Route

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Cited by 6 •

2016

A protocol for the preparation of novel zeolites by the ADOR (Assembly-Disassembly-Organization-Reassembly) synthetic route is presented.

Research

JoVE Journal - Engineering
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Two-way Valorization of Blast Furnace Slag: Synthesis of Precipitated Calcium Carbonate and Zeolitic Heavy Metal Adsorbent

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Cited by 6 •

2017

A protocol for the parallel production of precipitated calcium carbonate and zeolitic material from blast furnace slag via mineral carbonation and alkaline hydrothermal conversion, respectively, is presented. The performance of the zeolitic material towards nickel adsorption is tested.

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JoVE Journal - Engineering
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Nanostructured Ag-zeolite Composites as Luminescence-based Humidity Sensors

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Cited by 9 •

2016

A protocol for the synthesis of moisture-responsive luminescent Ag-zeolite composites is described in this report.

Research

JoVE Journal - Chemistry

Organic Structure-directing Agent-free Synthesis for *BEA-type Zeolite Membrane

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Cited by 2 •

2020

A *BEA seed crystal was loaded on a porous α-Al2O3 support by the dip-coating method, and hydrothermally grown without using an organic structure-directing agent. A *BEA-type zeolite membrane having very few defects was successfully prepared by the secondary growth method.

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JoVE Journal - Engineering
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Adsorption Device Based on a Langatate Crystal Microbalance for High Temperature High Pressure Gas Adsorption in Zeolite H-ZSM-5

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Cited by 1 •

2016

A protocol for high-temperature and high-pressure gas adsorption measurements on zeolite H-ZSM-5 using an adsorption measurement device based on a langatate crystal microbalance is presented. Prior to the adsorption measurements, the synthesis of zeolite H-ZSM-5 on the langatate crystal microbalance sensor by the steam-assisted crystallization (SAC) method is demonstrated.

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