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Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques
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JoVE Journal Engineering
Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques

Characterization of Electrode Materials for Lithium Ion and Sodium Ion Batteries Using Synchrotron Radiation Techniques

DOI:
10.3791/50594-v

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10:03 min

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November 11, 2013

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, , , , , , , , ,
1Environmental Energy Technologies Division,Lawrence Berkeley National Laboratory, 2Department of Chemistry,University of Illinois at Chicago, 3Stanford Synchrotron Radiation Lightsource, 4Haldor Topsøe A/S, 5PolyPlus Battery Company

Chapters

  • 00:05Title
  • 02:19Characterization of Materials Using X-ray Powder Diffraction
  • 03:32Assessing Particle Morphologies Using Scanning Electron Microscopy (SEM)
  • 04:54Fabrication of Electrodes and Assembly of a Coin Cell
  • 07:10Performance of Experiment at the Synchrotron Facility
  • 08:12Results: In Situ X-ray Diffraction Data on Li/Lix [Ni0.45Mn0.45Co0.05Al0.05] O2 Cell
  • 09:20Conclusion

Summary

Automatic Translation

Automatic Translation

We describe the use of synchrotron X-ray absorption spectroscopy (XAS) and X-ray diffraction (XRD) techniques to probe details of intercalation/deintercalation processes in electrode materials for Li-ion and Na-ion batteries. Both in situ and ex situ experiments are used to understand structural behavior relevant to the operation of devices

Tags

Lithium Ion BatteriesSodium Ion BatteriesElectrode MaterialsSynchrotron RadiationX-ray DiffractionX-ray Absorption SpectroscopyIn Situ ExperimentsEx Situ ExperimentsIntercalation CompoundsTransition Metal OxidesPhosphatesRedox StatesPhase TransitionsLattice Parameters

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