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Assessment of Boron Doped Diamond Electrode Quality and Application to In Situ Modification of Local pH by Water Electrolysis
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JoVE Journal Chemistry
Assessment of Boron Doped Diamond Electrode Quality and Application to In Situ Modification of Local pH by Water Electrolysis

Assessment of Boron Doped Diamond Electrode Quality and Application to In Situ Modification of Local pH by Water Electrolysis

DOI:
10.3791/53484-v

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13:09 min

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January 06, 2016

•

,
1Warwick Electrochemistry and Interfaces Group, Department of Chemistry,University of Warwick

Chapters

  • 00:05Title
  • 01:12Acid Cleaning Boron Doped Diamond (BDD)
  • 02:23Contact Angle Measurement
  • 03:47BDD Material Characterization
  • 06:22Capacitance Measurements
  • 07:27Solvent Window and Redox Electrochemistry
  • 09:17pH Sensitive Iridium Oxide Film Deposition
  • 10:30Visual Assessment of Local pH Generation
  • 11:25Results: Typical Experimental Data for Characterization of High Quality Boron Doped Diamond Electrode Materials
  • 12:45Conclusion

Summary

Automatic Translation

Automatic Translation

A protocol is described for the characterization of the key electrochemical parameters of a boron doped diamond (BDD) electrode and subsequent application for in situ pH generation experiments.

Tags

Boron Doped DiamondElectrode QualityElectro-chemical AssessmentSolvent WindowCapacitanceReversibilityNon-diamond CarbonLocal PH ControlWater ElectrolysisContact AngleSurface Termination

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