/

/

Sulfate Separation by Selective Crystallization with a Bis-iminoguanidinium Ligand

JoVE Journal
Chemistry

A subscription to JoVE is required to view this content. Sign in or start your free trial.

JoVE Journal Chemistry

Sulfate Separation by Selective Crystallization with a Bis-iminoguanidinium Ligand

Sulfate Separation by Selective Crystallization with a Bis-iminoguanidinium Ligand

DOI:

10.3791/54411-v

•

08:01 min

•

September 08, 2016

•

Charles A. Seipp², Neil J. Williams³, Radu Custelcean

¹Chemical Sciences Division,Oak Ridge National Laboratory, ²Department of Chemistry,The University of Texas at Austin, ³Department of Chemistry,The University of Tennessee

Chapters

00:05Title
00:41In Situ Synthesis of 1,4-Benzene-bis(iminoguanidinium) Chloride Ligand and its Crystallization with Sulfate
01:46Ex Situ Synthesis of 1,4-Benzene-bis(iminoguanidinium) Chloride
03:13Sulfate Separation from Seawater and Lingand Recovery
04:51Determination of the Amount of Sulfate Removed by β Liquid Scintillation Counting
06:38Results: Sulfate Separation from Seawater and Ligand Syntheses and Recovery Yields
07:25Conclusion

Summary

Automatic Translation

A protocol for in situ aqueous synthesis of a bis(iminoguanidinium) ligand and its utilization in selective separation of sulfate is presented.

Tags

Keywords: Sulfate Separation Selective Crystallization Bis-iminoguanidinium Ligand In Situ Synthesis Ex Situ Synthesis Terephthalaldehyde Aminoguanidinium Chloride BBIG Chloride BBIG Sulfate Seawater Anion Separation Hydrophilic Anion Aqueous Solutions Vacuum Filtration Powder X-ray Diffraction

Article

Embed

ADD TO PLAYLIST

Usage Statistics

Related Videos

Preparation and Characterization of SDF-1α-Chitosan-Dextran Sulfate Nanoparticles

Synthesis of Ligand-free CdS Nanoparticles within a Sulfur Copolymer Matrix

Preparation of Biopolymer Aerogels Using Green Solvents

Capillary Electrophoresis to Monitor Peptide Grafting onto Chitosan Films in Real Time

Accessing Valuable Ligand Supports for Transition Metals: A Modified, Intermediate Scale Preparation of 1,2,3,4,5-Pentamethylcyclopentadiene

Syntheses, Crystallization, and Spectroscopic Characterization of 3,5-Lutidine N-Oxide Dehydrate

Synthesis of a Thiol Building Block for the Crystallization of a Semiconducting Gyroidal Metal-sulfur Framework

Separation of Aldehydes and Reactive Ketones from Mixtures Using a Bisulfite Extraction Protocol

Analyzing Protein Architectures and Protein-Ligand Complexes by Integrative Structural Mass Spectrometry

Electrophoretic Crystallization of Ultrathin High-performance Metal-organic Framework Membranes

Read Article