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Synthesis and Characterization of Fe-doped Aluminosilicate Nanotubes with Enhanced Electron Conductive Properties
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JoVE Journal Chemistry
Synthesis and Characterization of Fe-doped Aluminosilicate Nanotubes with Enhanced Electron Conductive Properties

Synthesis and Characterization of Fe-doped Aluminosilicate Nanotubes with Enhanced Electron Conductive Properties

DOI:
10.3791/54758-v

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09:34 min

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November 15, 2016

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, , , , ,
1Department of Applied Science and Technology,Politecnico di Torino, 2Department of Civil and Mechanical Engineering,Università degli Studi di Cassino e del Lazio Meridionale, 3Institute of Chemistry,Politecnico di Torino, 4Department of Chemistry & NIS Interdepartmental Centre,University of Turin, 5INSTM Unit of Torino-Politecnico,Politecnico di Torino

Chapters

  • 00:05Title
  • 01:23Synthesis of Imogolite Nanotubes (IMO NTs)
  • 03:29Post-synthesis Loading of IMO NTs with Fe (Fe-L-IMO)
  • 04:15Synthesis of IMO NTs Doped with 0.7 wt% Fe (Fe-0.70-IMO)
  • 05:29Transmission UV-Vis Spectroscopy of Dye Adsorption over Time
  • 06:48Results: The Effects of Fe Doping on IMO NTs
  • 08:18Conclusion

Summary

Automatic Translation

Automatic Translation

Here, we present a protocol to synthesize and characterize Fe-doped aluminosilicate nanotubes. The materials are obtained by either sol-gel synthesis upon addition of FeCl3•6H2O to the mixture containing the Si and Al precursors or by post-synthesis ionic exchange of preformed aluminosilicate nanotubes.

Tags

Keywords: Iron-doped Aluminosilicate NanotubesImogoliteSynthesisCharacterizationPhotocatalyticSemiconductorBand GapAluminum Tri-sec-butoxideTetraethyl OrthosilicatePerchloric AcidHydrothermalNanotube Formation

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