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Spark Plasma Sintering Apparatus Used for the Formation of Strontium Titanate Bicrystals
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JoVE Journal Engineering
Spark Plasma Sintering Apparatus Used for the Formation of Strontium Titanate Bicrystals

Spark Plasma Sintering Apparatus Used for the Formation of Strontium Titanate Bicrystals

DOI:
10.3791/55223-v

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11:17 min

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February 09, 2017

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,
1Department of Materials Science and Engineering,University of California, Davis

Chapters

  • 00:05Title
  • 00:50Strontium Titanate (SrTiO3) Single Crystal Sample Preparation
  • 01:54SrTiO3 Bicrystal Formation via a Spark Plasma Sintering (SPS) Apparatus
  • 03:44SrTiO3 Bicrystal Sample Preparation
  • 04:53TEM Sample Preparation via Focused Ion Beam (FIB) Milling
  • 09:08Results: Spark Plasma Sintering Apparatus-formed Strontium Titanate Bicrystals
  • 10:36Conclusion

Summary

Automatic Translation

Automatic Translation

A viable technique for the formation of strontium titanate bicrystals at high pressure and fast heating rate via the spark plasma sintering apparatus is developed.

Tags

Keywords: Spark Plasma SinteringStrontium Titanate BicrystalsGrain Boundary StructuresMisorientationCeramic ProcessingMicrostructure FormationSample PreparationDiamond Wire SawUltrasonic CleaningEtchingGraphite PaperGraphite DieUniaxial ForceThermocouple

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