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In Situ Characterization of Boehmite Particles in Water Using Liquid SEM
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JoVE Journal Chemistry
In Situ Characterization of Boehmite Particles in Water Using Liquid SEM

In Situ Characterization of Boehmite Particles in Water Using Liquid SEM

DOI:
10.3791/56058-v

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11:59 min

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September 27, 2017

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, , , , , ,
1Earth & Biological Sciences Directorate,Pacific Northwest National Laboratory

Chapters

  • 00:05Title
  • 01:19Mount the device and Use SEM/Focused Ion Beam (FIB) to Make Apertures on the SALVI Silicon Nitride Membrane Using FIB
  • 03:46Load SALVI with Liquid Samples
  • 04:58Conduct Liquid SEM Imaging and Element Analysis
  • 09:30Results: In Situ Imaging of Beohmite Particles in Liquid Using SEM
  • 10:39Conclusion

Summary

Automatic Translation

Automatic Translation

We present a procedure for real-time imaging and elemental composition analysis of boehmite particles in deionized water by in situ liquid Scanning Electron Microscopy.

Tags

Keywords: In Situ CharacterizationBoehmite ParticlesLiquid SEMMicrofluidic ModuleParticle Size And MorphologyHigh-vacuum SEMEnvironmental ChangesPolydispersed ParticlesLiquid Material AnalysisBiological SamplesSALVI DeviceCarbon CoatingMicrofluidic Device MountingSEM StageGroundingCharging EffectCarbon TapeCopper TapeSilicon Nitride MembranePDMS BlockHigh Vacuum Mode

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