Journal
/
Chemistry
/
Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines
JoVE Journal
Chemistry
A subscription to JoVE is required to view this content.  Sign in or start your free trial.
JoVE Journal Chemistry
Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines

Preparation of N-(2-alkoxyvinyl)sulfonamides from N-tosyl-1,2,3-triazoles and Subsequent Conversion to Substituted Phthalans and Phenethylamines

DOI:
10.3791/56848-v

•

10:42 min

•

January 03, 2018

•

, , , , , ,
1Chemistry Department,Hamilton College

Chapters

  • 00:05Title
  • 00:48Synthesis of N-Tosyl Triazole 2a:2-(1-tosyl-1H-1,2,3 triazol-4-yl)phenyl Methanol
  • 03:03Synthesis of N-(2-alkoxyvinyl)sulfonamide Phthalan 3a: (Z)-N-(isobenzofuran-1(3H)-ylidenemethyl)-4-methylbenzenesulfonamide
  • 04:14Synthesis of Phthalan 4: N-((1,3-dihydroisobenzofuran-1-yl)methyl)-4-methylbenzenesulfonamide
  • 05:34Synthesis of Phenylthylamine 5: N-(2-(hydroxymethyl)phenethyl)-4-methylbenzenesulfonamide
  • 07:29Synthesis of Ketal 6c: N-((1-(2-hydroxyethoxy)-1,3-dihydroisobenzofuran-1-yl)methyl)-4-methybenzenesulfonamide
  • 08:12Results: Characterization of N-(2-alkoxyvinyl)sulfonamides and Derivatives
  • 10:00Conclusion

Summary

Automatic Translation

Automatic Translation

Representative experimental procedures for the synthesis of N-(2-alkoxyvinyl)sulfonamides and subsequent conversion to phthalan and phenethylamine derivatives are presented in detail.

Tags

Keyword Extraction: N-(2-alkoxyvinyl)sulfonamidesN-tosyl-123-triazolesPhthalansPhenethylamines2-ethynylbenzyl AlcoholCopper-thiophene-carboxylateP-Toluenesulfonyl AzideMicrowave ReactorSilica GelFlash ChromatographyTriazole Product

Article

Embed

ADD TO PLAYLIST

Usage Statistics

Related Videos

check_url/56848?article_type=v

Nucleoside Triphosphates – From Synthesis to Biochemical Characterization
check_url/56848?article_type=v

Preparation and Characterization of SDF-1α-Chitosan-Dextran Sulfate Nanoparticles
check_url/56848?article_type=v

Preparation of Mica and Silicon Substrates for DNA Origami Analysis and Experimentation
check_url/56848?article_type=v

Preparation and Characterization of Individual and Multi-drug Loaded Physically Entrapped Polymeric Micelles
check_url/56848?article_type=v

Facile Preparation of 4-Substituted Quinazoline Derivatives
check_url/56848?article_type=v

Laboratory Production of Biofuels and Biochemicals from a Rapeseed Oil through Catalytic Cracking Conversion
check_url/56848?article_type=v

One-pot Microwave-assisted Conversion of Anomeric Nitrate-esters to Trichloroacetimidates
check_url/56848?article_type=v

Preparation and Characterization of C60/Graphene Hybrid Nanostructures
check_url/56848?article_type=v

The Effect of Ultraviolet Radiation on the Chemical Bath Deposition of Bis(thiourea) Cadmium Chloride Crystals and the Subsequent CdS Obtention
check_url/56848?article_type=v

Tuning Oxide Properties by Oxygen Vacancy Control During Growth and Annealing

Read Article