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Molten-Salt Synthesis of Complex Metal Oxide Nanoparticles
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JoVE Journal Chemistry
Molten-Salt Synthesis of Complex Metal Oxide Nanoparticles

Molten-Salt Synthesis of Complex Metal Oxide Nanoparticles

DOI:
10.3791/58482-v

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08:43 min

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October 27, 2018

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, , ,
1Department of Chemistry,University of Texas Rio Grande Valley, 2Radiochemistry Division,Bhabha Atomic Research Centre, 3School of Earth, Environmental, and Marine Sciences,University of Texas Rio Grande Valley

Chapters

  • 00:00Title
  • 00:33Preparation of Single-source Complex Precursor via a Coprecipitation Route, Preparation of Lanthanum and Hafnium Precursor Solution
  • 01:09Preparation of Diluted Ammonia Solution
  • 01:34Titration and Washing the Single Source Complex Precursor
  • 02:44Vacuum Filtration and Drying of Precursor
  • 03:10Molten-salt Synthesis of Lanthanum Hafnate NPs, Preparation of Salt and Precursor Mixture
  • 04:06Molten Salt Processing
  • 04:21Results: Representative Structural Analyses
  • 07:04Conclusion

Summary

Automatic Translation

Automatic Translation

Here, we demonstrate a unique, relatively low-temperature, molten-salt synthesis method for preparing uniform complex metal oxide lanthanum hafnate nanoparticles.

Tags

Keywords: Molten Salt SynthesisMetal Oxide NanoparticlesLanthanum Hafnium NanoparticlesPrecipitationAmmoniaVacuum FiltrationPotassium NitrateSodium NitratePrecursorGrinding

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