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Isolating Free Carbenes, their Mixed Dimers and Organic Radicals
 

Isolating Free Carbenes, their Mixed Dimers and Organic Radicals

Article DOI: 10.3791/59389-v
April 19th, 2019

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Summary April 19th, 2019

We present protocols for the isolation of stable heterocyclic carbenes. The synthesis of a cyclic (alkyl)(amino) carbene (CAAC) and an N-heterocyclic carbene (NHC) is demonstrated using filter cannulas and Schlenk technique. We furthermore present the synthesis of the related oxygen-sensitive, electron-rich mixed “Wanzlick dimer” and the reduced stable organic radical.

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