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DOI: 10.3791/60391-v
This article presents a protocol for studying the formation of hydrates influenced by nonionic surfactants at the interface of water droplets in cyclopentane. The method integrates a low-cost, programmable temperature regulator with visualization techniques and internal pressure measurements.
We present a protocol to study the formation of hydrates in the presence of nonionic surfactants on the interface of a water droplet submerged in cyclopentane. The protocol consists of building a low-cost, programmable, temperature regulator. The temperature control system is combined with visualization techniques and internal pressure measurements.
The protocol is applicable in studying the effect of surfactant inhibitors on hydrate crystals. It provides information on both the type of the crystal and the mechanism for inhibition. Attach a 19 gauge needle to a one milliliter glass syringe.
Rinse the needle and syringe three times with deionized water and then fill the syringe with deionized water. Next, fill the hydrate visualization cell with 25 milliliters of cyclopentane. Using the syringe, insert a droplet of deionized water at the bottom of the hydrate visualization cell.
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