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DOI: 10.3791/61572-v
This protocol details a facile, one-pot synthesis of manganese oxide (MnO) nanoparticles by thermal decomposition of manganese(II) acetylacetonate in the presence of oleylamine and dibenzyl ether. MnO nanoparticles have been utilized in diverse applications including magnetic resonance imaging, biosensing, catalysis, batteries, and waste water treatment.
Compared to other synthesis methods, thermal decomposition generates uniform metal oxide nano-particles with tight control over particle size, shape, and chemical composition. This technique is an easy one pot synthesis that uses three reagents, a metal precursor, an organic solvent and a stabilizer. It can produce different types of nano-particles including manganese oxide and iron oxide.
Demonstrating the procedure will be Celia Martinez De La Torre, a graduate research assistant in my laboratory. Before beginning an experiment, place a four neck 500 milliliter round bottom flask onto the heating mantle. And secure the middle neck with a metal claw clamp.
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