Last Syntese av CdSe / CDer Rod og tetrapoder nanokrystaller

* These authors contributed equally
Chemistry
 

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Manthiram, K., Beberwyck, B. J., Talapin, D. V., Alivisatos, A. P. Seeded Synthesis of CdSe/CdS Rod and Tetrapod Nanocrystals. J. Vis. Exp. (82), e50731, doi:10.3791/50731 (2013).

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Abstract

Materials

Name Company Catalog Number Comments
Sodium hydroxide, 98% Fisher BP359
Myristic acid, 99% Sigma Aldrich M3128
Methanol, 99.8% Fisher A412
Cadmium nitrate tetrahydrate, 99% Sigma Aldrich 20911 Highly toxic
Cadmium oxide (CdO), 99.99% Sigma Aldrich 202894 Highly toxic
1-Octadecene (ODE), 90% Sigma Aldrich O806 Technical grade
Selenium (Se), 100 mesh, 99.99% Sigma Aldrich 229865
Tri-n-octylphosphine (TOP), 97% Strem 15-6655 Air sensitive
Sulfur (S), 99.9995% Alfa Aesar 10343
Trioctylphosphine oxide (TOPO), 99% Strem 15-6661
N-Octadecylphosphonic acid (ODPA), 99% PCI Synthesis 104224
Methanol, anhydrous, 99.8% Sigma Aldrich 322415
Toluene, anhydrous, 99.8% Sigma Aldrich 244511
Chloroform, anhydrous, 99% Sigma Aldrich 288306
Acetone, 99.9% Fisher A949 Dried over 4Å sieves
Hexane, anhydrous, 95% Sigma Aldrich 296090
2-Propanol, anhydrous, 99.5% Sigma Aldrich 278475
Selenium dioxide, 99.999% Sigma Aldrich 204315
Oleic acid, 90% Sigma Aldrich 364525 Technical grade
Oleylamine, 70% Sigma Aldrich O7805 Technical grade
Propylphosphonic acid (PPA), 95% Sigma Aldrich 305685
Ethanol, anhydrous, 99.5% Sigma Aldrich 459836
Octylamine, 99% Sigma Aldrich O5802

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References

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