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1-Aryl-1H-pyrazole-5-aminlerin mikrodalga destekli hazırlanması
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1-Aryl-1H-pyrazole-5-aminlerin mikrodalga destekli hazırlanması

Article DOI: 10.3791/59896-v • 05:07 min • June 23rd, 2019
June 23rd, 2019 •
*1, *1, *1, 1
1Department of Chemistry and Biochemistry, California Polytechnic State University
* These authors contributed equally

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1-aril-1H-pyrazol-5-aminokarin, 1 M HCL 'de bir mikrodalga reaktörü kullanarak 3-amino ocrotononitril veya α-cyanoketone ile birlikte aril hidazin ile hazırlanır. En reaksiyonlar 10-15 dakika içinde yapılır ve saf ürün% 70-90 tipik izole verimleri ile vakum filtrasyon ile elde edilebilir.

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Kimya Sayı 148 pyrazole-5-aminler mikrodalga sentezi heteroc yeşil kimya cyclization fenilhidazin α-cyanoketone 3-aminocrotononitrile
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