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In situ FTIR Spectroscopy as a Tool for Investigation of Gas/Solid Interaction: Water-Enhanced CO2 Adsorption in UiO-66 Metal-Organic Framework
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Chemie
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JoVE Journal Chemie
In situ FTIR Spectroscopy as a Tool for Investigation of Gas/Solid Interaction: Water-Enhanced CO2 Adsorption in UiO-66 Metal-Organic Framework

In situ FTIR Spectroscopy as a Tool for Investigation of Gas/Solid Interaction: Water-Enhanced CO2 Adsorption in UiO-66 Metal-Organic Framework

DOI:
10.3791/60285-v

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11:38 min

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February 01, 2020

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, , , , , ,
1Institute of General and Inorganic Chemistry,Bulgarian Academy of Sciences, 2Institute of Physical Chemistry and Electrochemistry,Leibniz Universität Hannover, 3Bulgarian Academy of Sciences

Kapitel

  • 00:00Introduction
  • 00:54Making Self-supporting Pellets
  • 02:05Pretreatment of the Sample
  • 03:11Registering Sample Spectrum
  • 04:16Adsorption of CD3CN at Room Temperature
  • 06:07Adsorption of CO at 100 K
  • 07:47Ergebnisse
  • 10:54Conclusion

Summary

Automatische Übersetzung

Automatische Übersetzung

The use of FTIR spectroscopy for investigation of the surface properties of polycrystalline solids is described. Preparation of sample pellets, activation procedures, characterization with probe molecules and model studies of CO2 adsorption are discussed.

Tags

In Situ FTIR SpectroscopyGas/solid InteractionWater-enhanced CO2 AdsorptionUiO-66 Metal-organic FrameworkAdsorptionHeterogeneous CatalysisSensingSolid SurfacesInfrared CharacterizationSample PreparationPellet FormationVacuum/adsorption ApparatusSample ActivationProbe Molecules

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