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High-Temperature and High-Pressure In situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy

Article DOI: 10.3791/61794-v • 08:55 min • October 9th, 2020
October 9th, 2020 •
1, 2, 1, 1
1Pacific Northwest National Laboratory, 2Washington State University

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The molecular structures and dynamics of solids, liquids, gases, and mixtures are of critical interest to diverse scientific fields. High-temperature, high-pressure in situ MAS NMR enables detection of the chemical environment of constituents in mixed phase systems under tightly controlled chemical environments.

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High-Temperature High-Pressure In Situ Magic Angle Spinning Nuclear Magnetic Resonance Spectroscopy Non-destructive Method Controlled Temperatures Controlled Pressures Scientific Questions NMR Experiments Specialized Conditions Multi-nuclear Nature Ketolysis Geochemistry Biology Pre-treatment Solid Sample Quartz Sample Tube Isolation Valves Gas Isolation Valve Cool Furnace Treatment System Desired Sample Environment Antechamber NMR Rotor
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