Sieve Tray Column

A sieve tray column is a vertical mass-transfer device that separates components in a gas-liquid mixture, commonly through distillation or absorption. Inside the column, liquid flows across perforated trays while vapor rises through holes, creating bubbles that promote contact and transfer volatile or soluble components between phases. Tray spacing, hole size, vapor velocity, and liquid flow influence separation efficiency, while excessive vapor or insufficient liquid can cause flooding or weeping. Sieve tray columns are widely used in chemical and petrochemical processing to purify solvents, recover valuable compounds, and study vapor-liquid equilibrium and column performance.

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JoVE Science Education - Engineering

The Effect of Reflux Ratio on Tray Distillation Efficiency

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2023

Source: Kerry M. Dooley and Michael G. Benton, Department of Chemical Engineering, Louisiana State University, Baton Rouge, LA Tray and packed columns are both commonly used for distillation, absorption, and stripping separation operations.1,2 The goal of this experiment is to distill a mixture of alcohols (methanol, isopropanol) and water in a sieve tray column and examine how closely simple theories of distillation based on equilibrium assumptions are followed. Sieve trays provide maximum...

Using a Tray Dryer to Investigate Convective and Conductive Heat Transfer

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2023

Source: Michael G. Benton and Kerry M. Dooley, Department of Chemical Engineering, Louisiana State University, Baton Rouge, LA Dryers are utilized in numerous industrial processes. The function of a dryer is to use heat transfer processes to dry solids. A variety of dryer types exist. Adiabatic dryers use convection and direct contact with gases to dry solids, whereas non-adiabatic dryers use methods other than heated gas contact to dry1, including conduction, radiation, and radio frequency...

Column Chromatography - Student Protocol

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2020

Source: Lara Al Hariri and Ahmed Basabrain at the University of Massachusetts Amherst, MA, USA Column Chromatography of Food DyeExpand In this experiment, you'll use column chromatography to separate green food coloring into its component blue and yellow dyes, called erioglaucine and tartrazine. First, you'll use 95% ethanol to elute the dye with a weaker affinity for silica gel. Then, you'll flush the second dye from the column with water. To recover the purified dyes, you will collect each...

Column Chromatography

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2023

Source: Laboratory of Dr. Jimmy Franco - Merrimack College Column chromatography is one of the most useful techniques for purifying compounds. This technique utilizes a stationary phase, which is packed in a column, and a mobile phase that passes through the column. This technique exploits the differences in polarity between compounds, allowing the molecules to be facilely separated.1 The two most common stationary phases for column chromatography are silica gel (SiO2) and alumina (Al2O3), with...

Column Chromatography - Concepts

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2020

Column Chromatography Multiple techniques exist to purify and separate compounds in an organic chemistry laboratory. One of the most reliable separation techniques for microscale separations, where less than 10 grams of the compound is available for analysis, is column chromatography. This technique separates compounds in a mixture based on their physical properties, such as their solubility, polarity, hydrophobicity, size, and charge. Chromatography Basics The main components of any...

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