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微波辅助合成一锅 N -琥珀酰亚胺- 4 - [ 18 F] fluorobenzoate([ 18 F] SFB)
JoVE Journal
Biology
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JoVE Journal Biology
Microwave-assisted One-pot Synthesis of N-succinimidyl-4-[18F]fluorobenzoate ([18F]SFB)
DOI:

08:33 min

June 28, 2011

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Chapters

  • 00:05Title
  • 01:51Preparation for [18F]SFB Synthesis
  • 03:03[18F]SFB Synthesis
  • 04:44Preparation of Solid Phase Extraction (SPE)-purified [18F]SFB
  • 07:24Representative Results for the Microwave-assisted One-pot Synthesis of [18F]SFB
  • 08:10Conclusion

Summary

Automatic Translation

一个轻便,一锅煮合成N -琥珀酰亚胺- 4 - [<sup> 18</sup> F] fluorobenzoate([<sup> 18</sup> F] SFB)是基于非水,三步走放过程。利用微波加热,就可以完成整个过程在不到30分钟,或60分钟,进一步纯化制备高效液相色谱法。衰减校正(RCYs)放的产量分别为35-5%(N> 30)。

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