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JoVE Journal Chemistry
Preparation of Graphene-Supported Microwell Liquid Cells for In Situ Transmission Electron Microscopy
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Preparation of Graphene-Supported Microwell Liquid Cells for In Situ Transmission Electron Microscopy

Article DOI: 10.3791/59751-v • 08:30 min • July 15th, 2019
July 15th, 2019 •
*1, *1, 2, 3, 3, 1,2,4
1Electron Devices (LEB), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg, 2Fraunhofer Institute for Integrated Systems and Device Technology (IISB), 3Institute of Micro- and Nanostructure Research (IMN) and Center for Nanoanalysis and Electron Microscopy (CENEM), Department of Materials Science and Engineering, Friedrich-Alexander University Erlangen-Nürnberg, 4Power Electronics (LEE), Department of Electrical, Electronic and Communication Engineering, Friedrich-Alexander University Erlangen-Nürnberg
* These authors contributed equally

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Summary
Automatic Translation

A protocol for preparation of graphene-supported microwell liquid cells for in situ electron microscopy of gold nanocrystals from HAuCl4 precursor solution is presented. Furthermore, an analysis routine is presented to quantify observed etching and growth dynamics.

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Graphene-supported Microwell Liquid Cells In Situ Transmission Electron Microscopy Nano Features High Resolution Dynamic Processes Graphene Technology Silicon Technology EDX Spectroscopy Analytical Methods In Situ Observation Research Training Group Microscopy With Electrons X-rays Scanning Probes German Research Foundation Procedure Demonstration Wetting Tissue CVD Graphene PMMA Membrane DI Water Filter Paper Graphene PMMA Stack Fabricated Wells
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