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Journal
/
Engineering
/
透過型電子顕微鏡
で
の密閉セルガス反応の実施
JoVE Journal
Engineering
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Performing
In Situ
Closed-Cell Gas Reactions in the Transmission Electron Microscope
Please note that all translations are automatically generated.
Click here for the English version.
透過型電子顕微鏡
で
の密閉セルガス反応の実施
DOI:
10.3791/62174-v
•
14:21 min
•
July 24, 2021
•
Kinga A. Unocic
,
Dale K. Hensley
,
Franklin S. Walden
,
Wilbur C. Bigelow
,
Michael B. Griffin
,
Susan E. Habas
,
Raymond R. Unocic
,
Lawrence F. Allard
1
Center for Nanophase Materials Sciences
,
Oak Ridge National Laboratory
,
2
Protochips Inc.
,
3
Department of Materials Science & Engineering
,
University of Michigan
,
4
Catalytic Carbon Transformation & Scale-up
,
National Renewable Energy Laboratory
,
5
Materials Science & Technology Division
,
Oak Ridge National Laboratory
Chapters
00:00
Introduction
01:40
E-chip Preparation
05:10
Preparation of the CCGR-TEM Holder
06:23
Preparation of Experimental Setup
07:59
Residual Gas Analyzer (RGA) System
10:52
Running the Reaction
12:46
Representative Results
13:29
Summary
Summary
Automatic Translation
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Automatic Translation
ここでは、いくつかの一般的に使用されるサンプル調製方法を詳述しながら
、Situ
TEM閉細胞ガス反応実験を行うためのプロトコルを提示する。
Tags
In Situ
Closed-cell Gas Reaction
CCGR
Scanning Transmission Electron Microscopy
Catalysts
Structural Materials
Carbon Nanotubes
Real-time Analysis
Elevated Temperature
Atmospheric Pressure
Sample Preparation
Powder Deposition
Colloidal Suspension
E-chip
Mask
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