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JoVE Journal
Chemistry

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Characterizing Lewis Pairs Using Titration Coupled with In Situ Infrared Spectroscopy
 

Characterizing Lewis Pairs Using Titration Coupled with In Situ Infrared Spectroscopy

Article DOI: 10.3791/60745-v 07:49 min February 20th, 2020
February 20th, 2020

Kapitel

Summary

Here, we present a method for the observation of solution interactions between Lewis acids and bases by employing in situ infrared spectroscopy as a detector for titration under synthetically relevant conditions. By examining solution interactions, this method represents a complement to X-ray crystallography, and provides an alternative to NMR spectroscopy.

Tags

Keywords: Lewis Pairs Titration In Situ Infrared Spectroscopy Carbonyl Reactions Mechanistic Insight Solution Interactions Reaction Monitoring IR Spectroscopy Experimental Setup
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