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Performing In Situ Closed-Cell Gas Reactions in the Transmission Electron Microscope

Article DOI: 10.3791/62174-v • 14:21 min • July 24th, 2021
July 24th, 2021 •
1, 1, 2, 3, 4, 4, 1, 5
1Center for Nanophase Materials Sciences, Oak Ridge National Laboratory, 2Protochips Inc., 3Department of Materials Science & Engineering, University of Michigan, 4Catalytic Carbon Transformation & Scale-up, National Renewable Energy Laboratory, 5Materials Science & Technology Division, Oak Ridge National Laboratory

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Summary
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Here, we present a protocol for performing in situ TEM closed-cell gas reaction experiments while detailing several commonly used sample preparation methods.

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In Situ Closed-cell Gas Reactions Transmission Electron Microscope Scanning Transmission Electromicroscopy CCGR Elevated Temperatures Aggressive Environments Material Changes Catalysts Structural Materials Carbon Nanotubes Atmospheric Pressure Kinetic Information Atomic Scale Level Reaction Mechanisms Surface Reactions Site-specific Interfaces Atomic Resolution Images Experimental Techniques Sample Preparation Challenges
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